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CONTINUOUS PROCESS AND DEVICE FOR CHROMATOGRAPHIC SEPARATION OF MIXTURE OF AT LEAST THREE CONSTITUENTS INTO THREE PURIFIED EFFLUENT BY MEANS OF SINGLE SOLVENT AT TWO DIFFERENT TEMPERATURES AND/OR TWO DIFFERENT PRESSURE
CONTINUOUS PROCESS AND DEVICE FOR CHROMATOGRAPHIC SEPARATION OF MIXTURE OF AT LEAST THREE CONSTITUENTS INTO THREE PURIFIED EFFLUENT BY MEANS OF SINGLE SOLVENT AT TWO DIFFERENT TEMPERATURES AND/OR TWO DIFFERENT PRESSURE
Process and apparatus for continuous, fluid phase separation of a mixture of at least three constituents into three fractions. …??A so-called simulated countercurrent technique is employed in a separation column filled with a sorbent having six zones 6, 5, 4, 3, 2 and 1 with different functions and the sequence of following stages is carried out: so-called strong solvent S2 is introduced, an extract E2 containing strong solvent is removed, so-called weak solvent S1 is introduced. Extract containing weak solvent E1 is drawn off, the mixture to be separated is introduced, raffinate containing weak solvent R is drawn off, rinsing solvent (S1) is introduced, a stream Rcy is recycled alternately towards the feed of the strong solvent S2 and then towards the feed of the weak solvent S1. A stream originating from the zone 6 is conveyed alternately towards an exit for extract containing strong solvent E2 and then towards the entry of the fifth zone. The various feeds and draw-offs are synchronously moved forward at regular intervals through the column. …??Application especially to the separation of glucose, xylose and arabinose and to the separation of para-xylene, of ortho-xylene and meta-xylene and of ethylbenzene. …IMAGE…
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