首页> 外国专利> METHOD FOR QUANTITATIVE DETERMINATION OF FRUCTOSE IN BEVERAGES, PREFERABLY IN SOUR MILK DRINKS, CONTAINING UP TO 50 OF AMERICAN ARTICHOKE PROCESSING PRODUCTS

METHOD FOR QUANTITATIVE DETERMINATION OF FRUCTOSE IN BEVERAGES, PREFERABLY IN SOUR MILK DRINKS, CONTAINING UP TO 50 OF AMERICAN ARTICHOKE PROCESSING PRODUCTS

机译:饮料中果糖含量的定量测定方法,主要用于酸牛奶饮料中,含量最高可达50%的美国中风加工产品

摘要

FIELD: analytical methods in food industry. SUBSTANCE: invention relates to electrochemical methods of analysis of carbohydrates, in particular to potentiometric method for quantitative determination of fructose (reducing sugar), which can be used as chemico-technological control of fructose in milk industry. Method consists in that a sample to be analyzed is neutralized with 30% sodium hydroxide solution to pH 9.00-9.20 and then added to 0.00125 M sodium tetraborate reagent solution at ratio 1:4 and pH of mixture is measured potentiometrically. To calculate fructose concentration (Cx), difference between pH of reagent solution and pH of reagent solution-sample mixture (&Dgr;pH) as well as difference between pH of reagent solution and pH of reagent solution-sour milk base mixture (&Dgr;pHф,) are measured and fructose concentration is calculated from equation: Cx = 1.12(&Dgr;pH-&Dgr;pHф)) wherein coefficient of proportionality 1.12 is found experimentally. Value of &Dgr;pHф varies between 0.12 and 0.23. Fructose determination range is 0.05-0.5 g/100 cu.cm. EFFECT: increased determination accuracy. 3 cl, 1 dwg, 1 tbl, 4 ex
机译:领域:食品工业中的分析方法。本发明涉及碳水化合物的电化学分析方法,尤其涉及定量测定果糖(还原糖)的电位法,该方法可用于牛奶工业中果糖的化学技术控制。方法在于,将待分析的样品用30%的氢氧化钠溶液中和至pH值9.00-9.20,然后以1:4的比例添加到0.00125 M的四硼酸钠试剂溶液中,并用电位法测量混合物的pH值。要计算果糖浓度(Cx),试剂溶液的pH值与试剂溶液-样品混合物的pH值之间的差异(& pH)以及试剂溶液的pH值和试剂溶液-酸乳基混合物的pH值之间的差异(&pH; ,测量果糖浓度,并从等式计算果糖浓度:Cx = 1.12(& pH-&pHф),其中比例系数为1.12。 pH值在0.12至0.23之间变化。果糖的测定范围是0.05-0.5 g / 100cu.cm。效果:提高测定精度。 3 cl,1 dwg,1 tbl,4 ex

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