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PREPARATION METHOD OF COLLOID COMPOSITION CONTAINING IRON OXIDE NANOPARTICLES AND COLLOID SOLUTION PREPARED BY THE METHOD

机译:包含氧化铁纳米粒子的胶体组合物的制备方法及该方法制备的胶体溶液

摘要

PURPOSE: A method for preparing a colloid solution containing iron oxide nanoparticles and a colloid solution prepared by the method are provided, to obtain a colloid solution containing iron oxide nanoparticles which is transparent, stable and highly dispersive and is free from precipitation. CONSTITUTION: The method comprises the steps of dissolving a surfactant in an organic solvent to prepare a surfactant solution; mixing an iron salt aqueous solution and the surfactant solution homogeneously to prepare an emulsion; mixing a basic solution and the surfactant solution homogeneously to prepare a basic mixture solution; and mixing the emulsion and the basic mixture solution. Preferably the surfactant is at least one anionic surfactant selected from the group consisting of sodium dodecyl sulfate, sodium bis(2-ethylhexyl)sulfosuccinate, dodecyl benzenesulfonic acid, sodium dioctyl sulfosuccinate, sodium alkyl phenol ether sulfonate and sodium alkyl sulfonate; the iron salt is at least one selected from the group consisting of iron sulfate, FeCl2, FeCl3, iron nitrate, pentacarbonyl iron, iron acetate, iron oxalate and iron ammonium sulfate; and the basic material of the basic solution is at least one selected from the group consisting of NaOH, KOH, LiOH, tetramethyl ammonia, ammonia and sodium carbonate.
机译:目的:提供一种制备含氧化铁纳米颗粒的胶体溶液的方法及通过该方法制备的胶体溶液,以得到一种透明,稳定,高度分散且无沉淀的含氧化铁纳米颗粒的胶体溶液。组成:该方法包括以下步骤:将表面活性剂溶解在有机溶剂中以制备表面活性剂溶液。将铁盐水溶液和表面活性剂溶液均匀混合以制备乳液。将碱性溶液和表面活性剂溶液均匀混合以制备碱性混合物溶液。并将乳液和碱性混合物溶液混合。优选地,表面活性剂是选自十二烷基硫酸钠,双(2-乙基己基)磺基琥珀酸钠,十二烷基苯磺酸钠,二辛基磺基琥珀酸钠,烷基酚醚磺酸钠和烷基磺酸钠的至少一种阴离子表面活性剂;铁盐是选自硫酸铁,FeCl 2,FeCl 3,硝酸铁,五羰基铁,乙酸铁,草酸铁和硫酸铁铵中的至少一种;碱性溶液的碱性物质是选自NaOH,KOH,LiOH,四甲基氨,氨和碳酸钠中的至少一种。

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