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Process for making a solution of copolymers of maleic anhydride and alkyl vinyl ether in isopropyl acetate of high specific viscosity and at a high solids level
Process for making a solution of copolymers of maleic anhydride and alkyl vinyl ether in isopropyl acetate of high specific viscosity and at a high solids level
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机译:制备马来酸酐和烷基乙烯基醚的共聚物在乙酸异丙酯中的高比浓粘度和高固体含量的溶液的方法
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摘要
A process for making a solution of a copolymer of maleic anhydride (MA) and methyl vinyl ether (MVE) monomers the specific viscosity (SV) of the product being about 2.5-6, preferably 3-5, indicating a weight average molecular weight of substantially above one million, preferably above 1.5 million and a solids content of about 20-45%, preferably 30-40, in isopropyl acetate (IPAc), solvent includes the steps of (a) precharging part of MVE in IPAc into a reactor heated to about 50-90° C., and then (b) feeding (i) a solution of MA in IPAc, (ii) the rest of MVE, at a mole ratio of MA:MVE of 1:≧1.5 to 1:3, preferably 1:2.4, and (iii) a free radical initiator dissolved in IPAc, in an amount of 0.02-0.3%, preferably 0.05-0.2%, based on total monomers, into the reactor over time. Powders of such MA/MVE copolymers are made by removing the solvent from the solution.
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