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METHOD FOR PREPARING OF ION-EXCHANGE TYPE NANO-LITHIUM MANGANESE OXIDE POWDER ADSORBENT BY GEL PROCESS

机译:凝胶法制备离子交换型纳米锂锰氧化物粉体吸附剂的方法

摘要

The method comprising stirring a mixture of 1.67 to;: - The present invention in an ion exchange-type nano using the gel method, the lithium compound and the manganese compound solution solution relates to a method for producing a lithium manganese oxide powder sorbent molar ratio 1.33 The step of gelling the mixture was added a solution of tartaric acid or citric acid solution was added dropwise a mixture; Drying the gelled mixture; Heat-treating the dried mixture; And the step of acid treatment for the heat-treated mixture; Ion exchange type nano-containing-provides a process for the preparation of lithium manganese oxide powder adsorbent.; According to the present invention, subsequent to using the gel method by preparing the adsorbent powder of nano-size, it is possible to secure a more lithium adsorbed reactive site to improve the specific surface area and pore volume of the adsorbent powder, the heat treatment and acid treatment the lithium ion exchange method with the step can be selectively produced an effective adsorbent in powdered lithium ion sieve type capable of absorption / desorption with.
机译:该方法包括将1.67的混合物搅拌至::-使用凝胶法的离子交换型纳米中的本发明,锂化合物和锰化合物溶液溶液涉及一种制备锂锰氧化物粉末吸附剂摩尔比的方法1.33在使混合物胶凝的步骤中加入酒石酸溶液或柠檬酸溶液逐滴加入混合物;干燥胶凝的混合物;对干燥的混合物进行热处理;以及将酸处理的步骤用于热处理过的混合物;含离子交换型纳米颗粒提供了制备锂锰氧化物粉末吸附剂的方法。根据本发明,在通过使用凝胶法通过制备纳米尺寸的吸附剂粉末之后,可以确保更多的锂吸附的反应位点,以改善吸附剂粉末的比表面积和孔体积,热处理通过该步骤的锂离子交换法,可以选择性地制备有效的吸附剂,该吸附剂具有粉末状的锂离子筛型,可以吸收/解吸。

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