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A method for isolating and concentrating the fat-soluble vitamins and provitamins, growth factors and animal and plant hormones that are present in the waste and by-products of animal and vegetable products
A method for isolating and concentrating the fat-soluble vitamins and provitamins, growth factors and animal and plant hormones that are present in the waste and by-products of animal and vegetable products
1.method u0432u044bu0434u0435u043bu0435u043du0438u00a0 valuable product from u0441u044bu0440u044cu00a0, which includes training u0441u044bu0440u044cu00a0 containing one or more u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds and one or more u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds where one or more u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds contain one or more compounds in the form of a free acid and / or soap, interaction u043eu043cu044bu043bu00a0u0435u043cu043eu0433u043e componentcontaining one or more compounds in the form of a free acid and / or soap with metal u043cu044bu043bu043eu043eu0431u0440u0430u0437u0443u044eu0449u0438u043c compound to obtain a first product containing the metal soap, and one or more u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds, u043fu0435u0440u0435u0433u043eu043du043au0443 metal washing mixture and one or more u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds with the formation of u0434u0438u0441u0442u0438u043bu043bu0438 u0440u043eu0432u0430u043du043du043eu0433u043e product containing at least a part of the u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compoundsand the residue containing the metal soap.;2. method for p.1, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0, raw materials selected from the group u0441u043eu0441u0442u043eu00a0u0449u0435u0439 of u043fu0435u043du0438u0441u0442u043eu0439 mass u043eu0431u0440u0430u0437u0443u044eu0449u0435u0439u0441u00a0 surface black u0449u0435u043bu043eu043au0430 u0442u0430u043bu043bu043eu0432u043eu0433u043e, soap oil, raw u0442u0430u043bu043bu043eu0432u043eu0433u043e ma smi, peck u0442u0430u043bu043bu043eu0432u043eu0433u043e oils, butter, sugar cane residue after extraction, u0443u0434u0430u043bu0435u043du0438u00a0 resin and refining of oils and fats, fatty acids and residues from the distillation. few easy questions ethers, u0434u0435u0437u043eu0434u043eu0440u0438u0440u043eu0432u0430u043du043du044bu0445 u0434u0438u0441u0442u0438u043bu043bu00a0u0442u043eu0432 vegetable oils.soybean oil, rice bran oil, fat from the liver of shark u0433u043eu0432u00a0u0436u044cu0435u0433u043e fat coffee oil, cod liver oil, cod liver oil from the oil, wheat sprouts, oil u0440u043eu0441u0442u043au043e in corn, palm oil, oil and oil u0430u043du0434u0438u0440u043eu0431u044b remnants of the tomato.;3. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, so that the metal u043cu044bu043bu043eu043eu0431u0440u0430u0437u0443u044eu0449u0435u0435 compound selected from the group u0441u043eu0441u0442u043eu00a0u0449u0435u0439 of oxides, sulphate, u0433u0438u0434u0440u043eu043au0441u0438u0434u043eu0432, carbonates and chlorides zinc, iron, manganese, u043cu0430u0433u043du0438u00a0, u043au0430u043bu044cu0446u0438u00a0 and u0430u043bu044eu043cu0438u043du0438u00a0.;4. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, so that the valuable product is selected from the group u0441u043eu0441u0442u043eu00a0u0449u0435u0439 of u043fu0440u043eu0432u0438u0442u0430u043cu0438u043du043eu0432, growth factors, flavonoids, u0441u0442u0435u0440u043eu043bu043eu0432, u043bu0438u043fu043eu043fu0440u043eu0442u0435u0438u043du043eu0432, u0441u0442u0438u043bu044cu0431u0435u043du043eu0432, v vitamins, fatty alcohols and paraffin, u0434u0438u0442u0435u0440u043fu0435u043du043eu0432 u0442u0440u0438u0442u0435u0440u043fu0435u043du043eu0432, fatty acids, steroids, and u0441u043cu043eu043bu00a0u043du044bu0445 acids.;5. method for p.1, u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0, a valuable product is selected from the group u0441u043eu0441u0442u043eu00a0u0449u0435u0439 of u0442u043eu043au043eu0444u0435u0440u043eu043bu043eu0432, u0442u043eu043au043eu0442u0440u0438u0435u043du043eu043bu043eu0432, contains vitamin a, vitamin k, vitamin d, u0441u043au0432u0430u043bu0435u043du0430, u043eu0440u0438u0437u0430u043d hola, u043bu0438u043au043eu043fu0435u043du0430, u0446u0435u0440u0438u043bu043eu0432u043eu0433u043e alcohol, u043bu0438u0433u043du043eu0446u0435u0440u0438u043bu043eu0432u043eu0433u043e u0431u0435u0433u0435u043du0438u043bu043eu0432u043eu0433u043e alcohol, alcohol, u043au0430u043du0438u0444u043eu043bu044cu043du044bu0445 alcohols, u043au0430u043du0438u0444u043eu043bu044cu043du044bu0445 u0430u043bu044cu0434u0435u0433u0438u0434u043eu0432, u043bu0430u0431u0434u0430u043du043eu0432, u0441u0438u0442u043eu0441u0442u0435u0440u043eu043bu0430, u0441u0442u0438u0433u043cu0430u0441u0442u0430u043du043eu043bu0430, u043au0430u043cu043fu0435u0441u0442u0435u0440u043eu043bu0430, u043au0430u043cu043fu0435u0441u0442u0430u043du043eu043bu0430, u0446u0438u043au043bu043eu0430u0440u0442u0435u043du043eu043bu0430 3.5 u0441u0442u0438u0433u043cu0430u0441u0442u0430u0434u0438u0435u043d - 7 - sheu0441u0435u0440u0440u0430u0442u0435u043du0434u0438u043eu043bu0430, u0441u043au0432u0430u043bu0435u043du0430; u043fu0440u0435u043du043eu043bu043eu0432, u0434u0438u043cu0435u0442u0438u043bu043eu0432u043eu0433u043e air trans u0434u0438u043eu043au0441u0438u0441u0442u0438u043bu044cu0431u0435u043d, u0430u0431u0438u0435u0442u0438u043du043eu0432u043eu0439 u0434u0435u0433u0438u0434u0440u043eu0430u0431u0438u0435u0442u0438u043du043eu0432u043eu0439 u043du0435u043eu0430u0431u0438u0435u0442u0438u043du043eu0432u043eu0439 acid, acid, acid, u0438u0437u043eu043fu0438u043cu0430u0440u043eu0432 oh u043fu0438u043cu0430u0440u043eu0432u043eu0439 u043fu0430u0443u043bu0441u0442u0440u0438u043du043eu0432u043eu0439 acid, acid, acid, u043eu043bu0435u0438u043du043eu0432u043eu0439 u043bu0438u043du043eu043bu0435u0432u043eu0439 acid, acid, acid and u0441u0442u0435u0430u0440u0438u043du043eu0432u043eu0439 u043fu0430u043bu044cu043cu0438u0442u0438u043du043eu0432u043eu0439 acid.;6. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, so that further includes the interaction u0441u044bu0440u044cu00a0 with u043du0430u0442u0440u0438u0435u0432u044bu043c or u043au0430u043bu0438u0435u0432u044bu043c ground u0434u043bu00a0 u043eu043cu044bu043bu0435u043du0438u00a0 containing free acid. u044bu043bu00a0u0435u043cu044bu0445 compounds with the formation of the mixture containing u043eu043cu044bu043bu0435u043du043du044bu0435 u0441u043eu0435u0434u0438u043du0435u043du0438u00a0 and u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0435 u0441u043eu0435u0434u0438u043du0435u043du0438u00a0 prior to reaction with the formation of the first u043fu0440u043eu0434u0443 acts.;7. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 2, so that the u043du0430u0442u0440u0438u0435u0432u043eu0435 or u043au0430u043bu0438u0435u0432u043eu0435 base selected from the group u0441u043eu0441u0442u043eu00a0u0449u0435u0439 of hydroxide and the hydroxide u043du0430u0442u0440u0438u00a0 u043au0430u043bu0438u00a0.;8. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.6, however, that further includes hydrolysis of complex esters in raw materials in collaboration with the u043du0430u0442u0440u0438u0435u0432u044bu043c or u043au0430u043bu0438u0435u0432u044bu043c basis.;9. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.6, however, that further includes the addition of mineral acid to at least part of the u043eu043cu044bu043bu0435u043du043du044bu0445 compounds with the formation of u043fu043eu0434u043au0438u0441u043bu0435u043du043d oh the mixture prior to the reaction with the formation of the first product.;10. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.6, however, that further includes u043fu0435u0440u0435u0433u043eu043du043au0443 acidified mixture to obtain residue containing one or more u043du0435u043bu0435u0442u0443u0447u0438u0445 compounds, and dr. u0438u0441u0442u0438u043bu043bu0438u0440u043eu0432u0430u043du043du043eu0433u043e product containing one or more u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds and one or more u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds prior to reaction with the formation of the the product.;11. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, however, that further includes u043fu0435u0440u0435u0433u043eu043du043au0443 u0441u044bu0440u044cu00a0 obtaining residue containing one or more u043du0435u043bu0435u0442u0443u0447u0438u0445 compounds, and u0434u0438u0441u0442u0438u043bu043bu0438u0440u043eu0432u0430u043d the main product containing one or more u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds and one or more u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds prior to reaction with the formation of the first product.;12. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, however, that further includes hydrolysis of complex esters in raw material to obtain u0441u044bu0440u044cu00a0 containing u0433u0438u0434u0440u043eu043bu0438u0437u043eu0432u0430u043du043du044bu0435 esters, u043fu0440u0435u0434u0448u0435u0441 u0442u0432u0443u044eu0449u0438u0439 reactions with the formation of the first product.;13. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.12, so that hydrolysis u043eu0441u0443u0449u0435u0441u0442u0432u043bu00a0u044eu0442 by u043eu0431u044au0435u0434u0438u043du0435u043du0438u00a0 u0441u044bu0440u044cu00a0 with water under pressure at elevated temperatures.;14. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.12, however, that further includes u043fu0435u0440u0435u0433u043eu043du043au0443 u0441u044bu0440u044cu00a0 containing u0433u0438u0434u0440u043eu043bu0438u0437u043eu0432u0430u043du043du044bu0435 esters to obtain the balance containing one or more u043du0435u043bu0435u0442u0443u0447u0438u0445 compounds, and u0434u0438u0441u0442u0438u043bu043bu0438u0440u043eu0432u0430u043du043du043eu0433u043e product containing one or more u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds and one or more u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds, u043fu0440u0435u0434u0448u0435u0441u0442u0432u0443u044eu0449 other reactions with the formation of the first product.;15. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, however, that further includes a processing u0441u044bu0440u044cu00a0 u0434u043bu00a0 u0443u0434u0430u043bu0435u043du0438u00a0 u0437u0430u0433u0440u00a0u0437u043du0435u043du0438u0439 and / or u043du0435u043bu0435u0442u0443u0447u0438u0445 compounds prior to reaction with the education of the first product.;16. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, so that the first product u00a0u0432u043bu00a0u0435u0442u0441u00a0 essentially dry.;17. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, however, that further includes processing the first product u0434u043bu00a0 u0443u0434u0430u043bu0435u043du0438u00a0 water pre refining u0434u043bu00a0 u043eu0442u0434u0435u043bu0435u043du0438u00a0 at least part of the u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds from metal washing.;18. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.17, so that removal of water u043eu0441u0443u0449u0435u0441u0442u0432u043bu00a0u044eu0442 by u0438u0441u043fu0430u0440u0435u043du0438u00a0 in a thin film u0434u0435u043au0430u043du0442u0430u0446u0438u0438 and / or u0446u0435u043du0442u0440u0438u0444u0443u0433u0438u0440u043eu0432u0430u043du0438u00a0.;19. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, however, that further includes u043fu0435u0440u0435u0433u043eu043du043au0443 or warming of one or more compounds selected from the group u0441u043eu0441u0442u043eu00a0u0449u0435u0439 from light, medium light fractions and water from the first product, the pre refining u0434u043bu00a0 u043eu0442u0434u0435u043bu0435u043du0438u00a0 at least part of the u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds from metal washing.;20. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, so that the distilled product containing at least a part of the u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds, further subjected to refining with image u043eu0432u0430u043du0438u0435u043c second u0434u0438u0441u0442u0438u043bu043bu0438u0440u043eu0432u0430u043du043du043eu0433u043e product and the second balance and, thus, further purification and / or allocate u043du0435u043eu043cu044bu043bu00a0u0435u043cu044bu0445 compounds.;21. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.20, however, that further includes a second u0434u0438u0441u0442u0438u043bu043bu0438u0440u043eu0432u0430u043du043du043eu0433u043e u0441u0442u0435u0440u043eu043bu043eu0432 crystallization of the product.;22. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 1, however, that further includes the acidification of containing metal soap, the formation of their respective free u043au0438u0441u043b from the.;23. method for u043eu0442u043bu0438u0447u0430u044eu0449u0438u0439u0441u00a0 p.22, however, that further includes u043fu0435u0440u0435u0433u043eu043du043au0443 free acids.
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