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Synthesis of nickel-diamond composite powders by electroless plating method

机译:化学镀法合成镍-金刚石复合粉

摘要

The invention according to the electroless nickel plating method-relates to a composite diamond powder production method, and its object is continuous and uniform and the composition required for the excellent adhesion of the abrasive coating has excellent wear resistance 40-60wt% nickel the diamond particles of nickel coated on the surface - to provide an electroless nickel plating method for establishing a diamond composite powder manufacturing technology ; configuration of the present invention are synthetic diamond particles according to the method for manufacturing the composite powder of the nickel coating, screen sensitive to the surface of the synthetic diamond particles used as a core with SnCl 2 treatment on the surface, and PdCl 2 and pretreatment steps to enable processing by, NiSO 4 6H 2 O, Na acetate and Acetic the acid dissolves nickel sulfate salt solution which was charged with the pretreated diamond heated in the reaction vessel (reaction bath) to a predetermined temperature step in and, when it reaches the set reaction temperature Sodium hypophosphate and changes in the color of the solution by supplying a reducing agent containing Citric acid at a constant speed and through a reduction step of reacting hydrogen gas does not occur up to the point features a method such that the nickel particles coated on the surface of diamond.
机译:根据化学镀镍方法的本发明涉及一种复合金刚石粉末的生产方法,其目的是连续且均匀的,并且磨料涂层的优异粘附性所需的组成具有优异的耐磨性:40-60wt%的金刚石颗粒镍。表面镀镍-为建立金刚石复合粉体制造技术提供一种化学镀镍方法;本发明的结构是根据制造镍涂层复合粉末的方法的合成金刚石颗粒,其对用作芯的合成金刚石颗粒的表面在SnCl 2 处理下对屏幕敏感。表面,PdCl 2 和预处理步骤,以便能够通过NiSO 4 6H 2 O,乙酸钠和乙酸进行处理,该酸可溶解硫酸镍盐在反应容器(反应槽)中加热了预处理过的金刚石的溶液中,将其加入到预定温度,并在达到设定的反应温度时加入次磷酸钠,并通过提供含柠檬酸的还原剂来改变溶液的颜色以恒定的速度通过反应的还原步骤和不发生氢气的反应,直至将镍颗粒涂覆在金刚石表面上为止。

著录项

  • 公开/公告号KR100545107B1

    专利类型

  • 公开/公告日2006-01-24

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20030069807

  • 发明设计人 안종관;김동진;정헌생;

    申请日2003-10-08

  • 分类号B22F1/02;

  • 国家 KR

  • 入库时间 2022-08-21 21:24:28

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