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Process for preparing fatty acid methyl esters by transesterification of triglycerides, particularly from rapeseed oil and apparatus for making the same

机译:通过甘油三酸酯的酯交换反应制备脂肪酸甲酯的方法,特别是从菜籽油中制备脂肪酸甲酯的方法及其制备设备

摘要

The present invention relates to a process for preparing fatty acid methyl esters by transesterification of triglycerides, particularly from rapeseed oil and apparatus for making the same wherein the process is characterized by separating residues of glycerin phase form ester phase by cooling the ester phase leaving a third reactor (4) within a cooler (5) down to 30 to 50 degC and than supplying thereof in a coagulator (6) at the inlet of which the glycerin phase from a second separator (7) is supplied along with the glycerin phase from a first separator (3) in such a ratio as to make the ratio of the glycerin phase to the ester phase in the coagulator (6) within the range of 1:3 to 3:1.
机译:本发明涉及一种通过甘油三酸酯的酯交换反应制备脂肪酸甲酯的方法,特别是从菜籽油制备甘油甲酯的方法,其特征在于该方法的特征是通过冷却酯相而将甘油相的残余物从酯相中分离出来,留下第三冷却器(5)中的反应器(4)降至30至50摄氏度,然后将其供应至凝结器(6),在凝结器(6)的入口处,第二分离器(7)的甘油相与来自第一分离器(3)的比例应使凝结器(6)中甘油相与酯相的比例在1∶3至3∶1的范围内。

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