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METHOD FOR INCREASING THE RELIABILITY OF THE RESULTS OF RESEARCH solid surface by atomic force microscopy

机译:原子力显微镜提高研究固体表面结果可靠性的方法

摘要

1. A method for increasing the reliability of the results of studies solid surface by atomic force microscopy, comprising the step of scanning the reference surface and the test samples, placed on the table scanner unit of an atomic force microscope, and comparing the results obtained, characterized in that the scanner unit table atomically force microscope first place produce a reference sample and the measurement of the amplitude curves at the intermittently-contact mode, and then removed the reference sample placed on Hosting Project nnom the sample table and carry out measurement of the amplitude curves at the same parameters as for the reference sample, comparing the values ​​of the angle of inclination of the linear part of the amplitude curve for the test sample and the angle of inclination of the amplitude curve for the reference sample, with a deviation value of the slope of the amplitude of the test sample curve angle the value of this parameter for a reference sample by more than 10% moisture produced the gaseous medium over the test sample as long as the divergence angle values ​​of n clone linear part of the amplitude curve for the test sample and the angle of inclination of the amplitude curve for the reference sample will be no more than 10%, and when the value of said humidifying gas medium is stopped. ! 2. A method according to claim 1, characterized in that a freshly cleaved pyrographite is used as a reference sample.
机译:1.一种用于通过原子力显微镜提高固体表面研究结果的可靠性的方法,该方法包括以下步骤:扫描参考表面和测试样品,将其置于原子力显微镜的台式扫描仪单元上,并比较所获得的结果,其特征在于,扫描仪单元表首先用原子力显微镜以间歇接触方式产生参考样品和振幅曲线的测量值,然后取出放置在主机项目上的参考样品,并进行样品测量在与参考样品相同的参数下的振幅曲线,将测试样品的振幅曲线的线性部分的倾斜角和参考样品的振幅曲线的倾斜角的值进行比较,测试样品曲线幅度的斜率的偏差值与参考样品的该参数的值相差更多只要测试样品的振幅曲线的n个克隆线性部分的发散角值和参考样品的振幅曲线的倾斜角为大于10%,并且当所述加湿气体介质的值停止时。 ! 2.根据权利要求1所述的方法,其特征在于,将新鲜裂解的烙铁矿用作参考样品。

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