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manufacturing method of m- toluene diamine or m- toluene diisocyanate

机译:间甲苯二胺或间甲苯二异氰酸酯的制造方法

摘要

Toluenediamine is produced and separated from by-products of the reaction by: a) hydrogenating dinitrotoluene in the presence of a catalyst, b) separating the catalyst, water and optionally solvent from the hydrogenation reaction mixture to give crude toluenediamine, and c) separating by distillation the crude toluenediamine in a separating wall column into at least four product streams P 1 , P 2 , P 3 and P 4 . The product stream P 1 is a stream containing low boilers. The product stream P 2 is a stream containing o-toluenediamine. The product stream P 3 is a stream containing m-toluenediamine. The product stream P 4 is a stream containing high boilers and m-toluenediamine.
机译:通过以下方法生产并从反应副产物中分离甲苯二胺:a)在催化剂存在下将二硝基甲苯氢化,b)从氢化反应混合物中分离出催化剂,水和任选的溶剂,得到粗甲苯二胺,c)通过在分离壁塔中将粗甲苯二胺蒸馏成至少四个产物流P 1,P 2,P 3和P 4。产物流P 1是包含低沸物的流。产物料流P 2是含有邻甲苯二胺的料流。产物料流P 3是含有间甲苯二胺的料流。产物物流P 4是包含高沸物和间甲苯二胺的物流。

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