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METHOD FOR PREPARATION OF MESOPOROUS ZEOLITE/MN OXIDE COMPOSITES, AND THE MESOPOROUS ZEOLITE/MN OXIDE COMPOSITES THEREBY

机译:制备介孔沸石/锰氧化物复合材料的方法及由此制备的介孔沸石/锰氧化物复合材料

摘要

PURPOSE: A porous zeolite and manganese oxide composite, a manufacturing method thereof and a removal agent of volatile organic compounds which include the same are provided to effectively absorb and remove volatile organic compounds and to mass produce zeolites by synthesizing zeolites using microwave in short time. CONSTITUTION: A manufacturing method of a porous zeolite and manganese oxide composite comprises the following steps: (1 step) mixing a porous carbonaceous mold with a manganese oxide precursor solution; (2 step) adding a zeolite precursor solution to the mixture and mixing; (3 step) irradiating the mixture with microwave and synthesizing zeolites; removing the carbonaceous mold by heat treating the synthesized zeolites; and (4 step) forming mesopores within the zeolites. The manganese oxide is dispersed in the zeolite having mesopores. [Reference numerals] (AA) Step of mixing a porous carbonaceous mold with a manganese oxide precursor solution(Step 1); (BB) Step of adding a zeolite precursor solution to the mixture of the step 1 and mixing(Step 2); (CC) Step of irradiating the mixture with microwave and synthesizing zeolites(Step 3); (DD) Step of thermally treating the zeolites synthesized from the step 3 and removing the carbonaceous mold(Step 4)
机译:用途:提供一种多孔沸石和氧化锰复合物,其制造方法以及包括该多孔沸石和氧化锰的挥发性有机化合物的去除剂,以有效地吸收和去除挥发性有机化合物,并通过在短时间内使用微波合成沸石来大量生产沸石。组成:一种多孔沸石与氧化锰复合材料的制造方法,包括以下步骤:(1)将多孔碳质模具与氧化锰前体溶液混合; (2步骤)向混合物中加入沸石前驱体溶液并混合; (3步骤)用微波辐照混合物,合成沸石;通过热处理合成沸石除去碳质霉菌; (4步骤)在沸石内形成中孔。氧化锰分散在具有中孔的沸石中。 [附图标记](AA)将多孔碳质模具与氧化锰前体溶液混合的步骤(步骤1); (BB)将沸石前体溶液添加至步骤1的混合物中并混合(步骤2)的步骤; (CC)用微波照射混合物并合成沸石的步骤(步骤3); (DD)热处理由步骤3合成的沸石并除去碳质铸模的步骤(步骤4)

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