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Energy dispersive X-ray fluorescence analyzer PORTABLE

机译:能量色散X射线荧光分析仪便携式

摘要

The apparatus relates to means for spectral analysis and X-ray studies designed to advantageously heavy chemical elements in laboratory and field conditions. The apparatus includes an outer housing with cover plate and the exit window, form a closed chamber defined within the housing ray source unit replaceable filters primary X-rays, the collimator of the primary x-ray energy dispersive detector, analog-to-digital converter energy dispersive detector signals in the fluorescence spectrum of the sample, the processing unit fluorescence spectrum, as well as software-based control unit and an external helium supply system into the housing. Used X-ray optical circuit type inversion probe "X-ray source - the fluorescence detector", the optical axis of the X-ray source, collimator and energy dispersive detector located in one plane, wherein the X-ray source with collimator mounted secured to the optical axis orthogonal to the exit window plane, and energy dispersive detector is mounted with the optical axis inclination providing for the exit window plane, preferably in the range of angles 30 ° -45 ° and visibility of the irradiated region of the sample. Technical result is a weak fluorescence of the sample flow change when changing the selection of the radiation angle in said angle range, elimination of the effect of an air layer on the measurement results. The problem of optimization of the conditions of excitation and fluorescence detection, increase the accuracy of measurements of light chemical elements in the sample, regardless of the structure and shape of the sample.; 1 bp 5 and ZP 4-f ly Fig.
机译:该设备涉及用于光谱分析和X射线研究的装置,其被设计为有利地在实验室和野外条件下重化学元素。该设备包括带盖板的外壳和出射窗,形成一个封闭腔室,该腔室限定在外壳射线源单元内,可更换滤光片一次X射线,一次X射线能量色散检测器的准直仪,模数转换器能量色散检测器在样品的荧光光谱,处理单元的荧光光谱以及基于软件的控制单元和外部氦气供应系统中发出信号。使用X射线光路型反转探头“ X射线源-荧光检测器”,将X射线源的光轴,准直仪和能量色散检测器放置在一个平面上,其中固定有准直仪的X射线源固定垂直于出射窗平面的光轴倾斜,并且能量分散检测器安装有提供出射窗平面的光轴倾斜度,最好在30°-45°的角度范围内,并且样品的照射区域可见。技术结果是,在所述角度范围内更改辐射角度的选择时,样品流量变化的荧光较弱,从而消除了空气层对测量结果的影响。优化激发和荧光检测条件的问题增加了样品中轻化学元素的测量精度,而与样品的结构和形状无关。 1 bp 5和ZP 4-fly图。

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