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RAMAN SPECTROSCOPY METHOD OF MEASURING MELAMINE CONTENTS IN DAIRY PRODUCTS HAVING DIFFERENT MATRIXES

机译:拉曼光谱法测定不同基质乳制品中的三聚氰胺含量

摘要

A raman spectroscopy method of measuring melamine contents in dairy products having different matrixes. The method includes: (a) establishing a database of characteristic curves of dairy products having different matrixes; (b) taking several copies of the dairy products having one certain unknown matrix and adding melamine standard solutions having different concentrations therein, to obtain a series of dairy product samples in which the relative concentrations of the melamine are known; (c) performing raman spectrum testing analysis and obtaining corresponding characteristic peak intensities to obtain a slope of the characteristic curve showing variation of the characteristic peak intensities with the relative concentrations of the melamine; (d) searching the database of step (a) using the slope of the characteristic curve of the dairy product samples to find a matching characteristic curve, and (e) calculating concentration of melamine in the dairy products by using the matched characteristic curve and the characteristic peak intensity.
机译:拉曼光谱法测量具有不同基质的乳制品中三聚氰胺含量。该方法包括:(a)建立具有不同矩阵的乳制品的特征曲线的数据库; (b)取几份具有一个未知基质的乳制品,并在其中加入不同浓度的三聚氰胺标准溶液,以获得一系列已知三聚氰胺相对浓度的乳制品样品; (c)进行拉曼光谱测试分析并获得相应的特征峰强度,以得到显示特征峰强度随三聚氰胺相对浓度变化的特征曲线的斜率; (d)搜索步骤(a)的数据库,使用乳制品样品的特征曲线的斜率找到匹配的特征曲线,以及(e)使用匹配的特征曲线和乳制品,计算乳制品中三聚氰胺的浓度特征峰强度。

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