METHOD FOR DETERMINING PAHS IN WATER USING LC/MS/MS TECHNIQUES, AFTER PREVIOUS SOLID-PHASE EXTRACTION () OF SAMPLES

摘要

The invention relates to a method for determining polycyclic aromatic hydrocarbons from water samples. According to the invention, the method comprises the solid-phase extraction of samples followed by the quick and selective analysis of the sample on a chromatographic column, at a temperature of 25...45°C, mobile phase gradient of HO/CHCN, a flow rate of 400...600 μ L/min, using an atmospheric pressure ionization source, at source and compound parameters corresponding to each of the assessed polycyclic aromatic hydrocarbon.