首页> 外国专利> METHOD OF OBTAINING SUPERHARD NANO-STRUCTURED MATERIAL FROM BOHR'S NITRIDE

METHOD OF OBTAINING SUPERHARD NANO-STRUCTURED MATERIAL FROM BOHR'S NITRIDE

机译:从玻尔的氮化物中获得纳米材料的方法

摘要

1. A method for producing a nanostructured superhard diamond-like forms of matter from boron nitride, comprising preparing mixtures of powders and sphalerite wurtzite modifications, molding and sintering them at high pressures, temperatures and exposure times determined partial transition conditions for wurtzite-form boron nitride to cubic without rekristallizatsii.2. A method according to claim 1, characterized in that, in order to obtain a material with high abrasion and impact resistance, are used polycrystalline powders sphalerite modification ultrafine zernom.3. A method according to claim 1, characterized in that the powder obtained by crushing sphalerite modification polycrystalline compacts synthesized at thermobaric treatment pyrolytic bora.4 nitride. A method according to claim 1, characterized in that the polycrystalline powders sphalerite modification is taken from the range 10-50 microns and the grain sizes therein do not exceed 0.5 mkm.5. A method according to claim 1, characterized in that the mixture of sphalerite and wurtzite modification prepared in ratios from 4: 1 to 2: 3 sootvetstvenno.6. A method according to claim 1, characterized in that the pressure parameters selected from the range of 6.5-8.5 GPa and the sintering temperature was selected from the range of 1500-1800 ° C.7. A method according to claim 1, characterized in that the holding time at the sintering temperature is from 20 to 60 seconds to achieve full density and compact partial preservation of wurtzite phase.
机译:1.一种由氮化硼制备纳米结构的超硬类金刚石形式的物质的方法,包括制备粉末和闪锌矿纤锌矿变体的混合物,在高压,高温和暴露时间下模压和烧结它们,确定了纤锌矿形式硼的部分转变条件。氮化物成立方,不需再结晶; 2。 2.根据权利要求1所述的方法,其特征在于,为了获得具有高耐磨性和耐冲击性的材料,使用了多晶粉末闪锌矿改性的超细钙锰矿。 2.根据权利要求1的方法,其特征在于,通过压碎闪锌矿变质多晶压坯而获得的粉末,所述压坯是在热压处理的热解四氮化硼中合成的。 2.根据权利要求1所述的方法,其特征在于,所述多晶粉末闪锌矿变质的范围为10-50微米,并且其中的晶粒尺寸不超过0.5mkm.5。 2.根据权利要求1所述的方法,其特征在于,闪锌矿和纤锌矿变质的混合物以4∶1至2∶3的比率制备。6。 2.根据权利要求1所述的方法,其特征在于,所述压力参数选自6.5-8.5GPa的范围,并且所述烧结温度选自1500-1800°C.7。 2.根据权利要求1所述的方法,其特征在于,在烧结温度下的保持时间为20至60秒,以实现纤锌矿相的全密度和紧凑的部分保存。

著录项

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号