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Aerogel useful for producing carbon aerogel by pyrolysis of the aerogel, comprises resorcinol-formaldehyde

机译:通过热解气凝胶可用于生产碳气凝胶的气凝胶,包括间苯二酚-甲醛

摘要

Aerogel comprises resorcinol-formaldehyde. The aerogel is at least partially elastically deformable. Independent claims are also included for: (1) a carbon aerogel, which is obtained by pyrolysis of the aerogel; and (2) producing the aerogel, comprising (i) preparing a solution containing distilled water, resorcinol, formaldehyde and sodium carbonate, (ii) adjusting the pH of the solution to 5.3-5.6, (iii) gelling at a temperature of 70-90[deg] C, (iv) cooling the gel to room temperature and washing with an aprotic organic solvent, (v) drying the gel at an elevated temperature, where the formaldehyde is present in a stoichiometric excess with respect to resorcinol, and the molar ratio of resorcinol and water is 0.006-0.01.
机译:气凝胶包含间苯二酚-甲醛。气凝胶是至少部分可弹性变形的。还包括以下方面的独立权利要求:(1)通过气凝胶的热解获得的碳气凝胶; (2)制备气凝胶,包括(i)制备包含蒸馏水,间苯二酚,甲醛和碳酸钠的溶液,(ii)将溶液的pH调整至5.3-5.6,(iii)在70- 90°C,(iv)将凝胶冷却至室温并用非质子有机溶剂洗涤,(v)在高温下干燥凝胶,其中甲醛相对于间苯二酚以化学计量过量存在,并且间苯二酚与水的摩尔比为0.006-0.01。

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