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PROCESS FOR PREPARING A CU-ZN-AL ALLOY AND A SHAPE MEMORY BLANK

机译:制备铜锌合金和形状记忆坯的过程

摘要

The invention relates to a process for preparing a Cu-Zn-Al alloy of higher shape memory characteristics, made of composite depositions on a substrate of various shapes, using the powder metallurgy-specific double-jet pulverization method. According to the invention, the process for preparing an alloy comprising 70% Cu, 26% Zn and 4% Al in mass percentage, obtained from highly pure starting materials, of 99.5%, includes the preparation of a Cu-Al smelt and disintegration thereof as very fine drops, under the action of a strong 99.9%-pure argon jet, whereinto Zn as powder is simultaneously injected, cooling and solidification of the pre-alloyed powders, followed by admixing 3% zinc stearate and cold-pressing the mixture, at a pressure of 300 MPa, sintering of the compacted products in furnaces, under a protective argon atmosphere, at a temperature of 960°C, for 2 hours, with slow cooling inside the furnace, followed by 15...20 cycles of hot plastic deformation by rolling at 800°C, with water cooling, a secondary thermal treatment of recrystallization at 920°C, for 15 min, with water cooling, the alloy as laminas being finally subjected to training by undergoing 10 charging-discharging-heating-cooling cycles, depending on the type of strain it will be subjected to.
机译:本发明涉及一种利用粉末冶金专用的双喷射粉碎方法,由在各种形状的基底上的复合沉积物制成的,具有较高形状记忆特性的Cu-Zn-Al合金的制备方法。根据本发明,由高纯度的原材料获得的以质量百分比计包含70%的Cu,26%的Zn和4%的Al的合金的制备方法包括Cu-Al熔体的制备及其分解。在强99.9%的纯氩射流的作用下,以微细滴的形式滴入锌粉,同时将预合金化的粉末冷却并固化,然后混合3%​​的硬脂酸锌并冷压混合物,在300 MPa的压力下,在保护性氩气气氛中,在960°C的温度下,在炉内将压实产品烧结2小时,然后在炉内缓慢冷却,然后进行15 ... 20周期的热循环在水冷条件下于800°C滚动轧制,在920°C二次结晶热处理,在水冷条件下进行15分钟塑性变形,最后对作为薄板的合金进行10次充放电-加热-冷却周期,取决于它将承受的应变类型。

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