首页> 外国专利> Hydrophilic Magnetic Resin with High Specific Area, Preparation Method Therefor and Application Method Thereof for Rapidly Extracting Phthalates in Water Body

Hydrophilic Magnetic Resin with High Specific Area, Preparation Method Therefor and Application Method Thereof for Rapidly Extracting Phthalates in Water Body

机译:高比表面积的亲水磁性树脂,其制备方法及其在水体中邻苯二甲酸酯的快速提取中的应用方法

摘要

Implementations herein relate to a method for extraction of phthalates using hydrophilic magnetic resins with high specific surface areas. The implementations relate to a technical field of preparation of resins for fast enrichment and separation of trace organics in water. By adding magnetic particles, precursor resins may be prepared using divinylbenzene, vinyl benzoate and glycidyl methacrylate copolymerization ester. After the cross-linking reaction, surface areas of the resins are increased and hydrolysis of the ester group in alkaline solution may be implemented to obtain high specific surface magnetic resins rich in hydroxyl groups. The resins have higher adsorptive capacity and selectivity to adsorb phthalates in water samples. Rapid extraction may be implemented using magnetic solid phase extraction rod to achieve enrichment and separation of phthalates in a large amount of water samples.
机译:本文的实施方式涉及使用具有高比表面积的亲水性磁性树脂提取邻苯二甲酸酯的方法。实施方式涉及用于快速富集和分离水中痕量有机物的树脂制备技术领域。通过添加磁性颗粒,可以使用二乙烯基苯,苯甲酸乙烯酯和甲基丙烯酸缩水甘油酯共聚酯制备前体树脂。在交联反应之后,树脂的表面积增加,并且可以在碱性溶液中进行酯基的水解以获得富含羟基的高比表面磁性树脂。该树脂具有更高的吸附能力和选择性,可以吸附水样中的邻苯二甲酸盐。可以使用磁性固相萃取棒进行快速萃取,以实现大量水样品中邻苯二甲酸酯的富集和分离。

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