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Method of fractional distillation of liquid mixtures and fractional distillation of liquids

机译:液体混合物的分馏和液体的分馏的方法

摘要

1. The method of fractional distillation of liquid mixtures by temperature-controlled evaporation at temperatures below the boiling point of each fraction, when the vapor pressure of the most volatile fraction substantially exceeds the vapor pressure of the fractions remaining in the mixture until the fraction is completely evaporated in a directed flow of neutral gas or vapor, which is inhibited the condenser at the condensation temperature of the selected fraction, then the temperature of the mixture is increased until the next fraction is intensively evaporated and completely evaporates, and so on until evaporation the last fraction, characterized in that the boiling point of the desired fraction is reduced by aerating the liquid mixture with finely dispersed bubbles of gas or steam, which initiate a chain reaction of activation of the boiling centers directly in the critical volume of the liquid mixture in the form of an upward boiling stream of compressible meta-fluid, which accelerates heat and mass transfer from the heater to the condenser , which is cooled with the next portion of the liquid mixture, and provide the supply with the gas of the condensed fraction in the distillation column y with gidrolovushkoy, the bottom of which is temporarily withdrawn heavier portion of the reflux liquid from the boiling mixture, and the gases and steam from the sealed collection of distillate was again directed to the boiling of the liquid jet smesi.2. The method according to claim 1, characterized in that the ascending boiling stream of the compressible metal fluid is created by electrolysis of the electrically conductive liquid mixture in an electrically conductive evaporator with a sponge metal electrode or a finely porous ceramic atomizer with a conductive electrode, and the gases are sent back to the boiling liquid
机译:1.当挥发性最高的馏分的蒸气压显着超过混合物中剩余馏分的蒸气压直至馏分达到沸点时,通过在低于每个馏分的沸点的温度下通过温度控制蒸发对液体混合物进行分馏的方法在中性气体或蒸气的定向流中完全蒸发,这在所选馏分的冷凝温度下被冷凝器抑制,然后升高混合物的温度,直到下一个馏分被强烈蒸发并完全蒸发,依此类推直到蒸发最后一个馏分,其特征在于,通过用细分散的气体或蒸汽气泡对液体混合物充气来降低所需馏分的沸点,这直接在液体混合物的临界体积内引发了沸腾中心活化的链式反应以可压缩的间流向上沸腾的形式加速将热量和质量从加热器传递到冷凝器,该冷凝器由另一部分液体混合物冷却,并在带有gidrolovushkoy的蒸馏塔y中为冷凝馏分的气体供气,该馏分的底部被暂时抽出来自沸腾混合物的回流液体的较大部分,以及来自密封馏出物收集的气体和蒸汽再次被引导至液体喷射管的沸腾。2。 2.根据权利要求1所述的方法,其特征在于,所述可压缩金属流体的上升沸腾流是通过在具有海绵金属电极的导电蒸发器或具有导电电极的细孔陶瓷雾化器中电解所述导电液体混合物而产生的,气体被送回沸腾的液体

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