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METHOD FOR X-RAY FLUORESCENCE DETERMINATION OF CONTENT OF IMPURITIES OF STRUCTURAL MATERIALS

机译:X射线荧光光谱法测定结构材料杂质含量的方法

摘要

FIELD: measuring equipment.;SUBSTANCE: invention consists in the fact that the X-ray fluorescence determination of the content of impurities of structural materials comprises measuring of intensities of analytical lines of controlled impurities in the group of samples of this material, additionally measures the intensity of analytical lines of impurities in the samples of standard reference material containing the same contaminants, results of these measurements, build calibration curves of the intensity of analytical lines of elements with an additional measurement is carried out with review of the spectrum of the investigated structural material and defining main structural element of the investigated filler material, additionally measuring the intensity of analytical lines of the elements controlled by impurities in the samples consisting that element, absorption factors and the slopes of calibration curves calculated for samples consisting of the average value of the content element in the reference calibration of test samples and the filler material of construction, then get the true content of impurities in the test structural material by multiplying the ratio of the conditional content slopes calibration curves in the reference and test materials on the relevant mathematical formulas.;EFFECT: enabling high-precision of X-ray fluorescence determination of impurities in a variety of materials.;1 cl, 1 dwg, 1 tbl
机译:技术领域:本发明在于以下事实:结构材料的杂质的X射线荧光测定包括测量该材料的样品组中受控杂质的分析线的强度,另外测量包含相同污染物的标准参照材料样品中杂质的分析线强度,这些测量结果,通过附加测量建立元素分析线强度的校准曲线,并查看了所研究结构的光谱材料并确定所研究填充材料的主要结构元素,另外测量样品中由杂质控制的元素的分析线强度,该元素包括元素,吸收系数和为样品计算的校准曲线的斜率,包括内容元素t在测试样品和建筑填充材料的参考校准中,通过将参考材料和测试材料中的条件含量斜率校准曲线的比率乘以相关的数学公式,得出测试结构材料中杂质的真实含量。效果:可以高精度X射线荧光测定各种材料中的杂质; 1 cl,1 dwg,1 tbl

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