首页> 外国专利> Method for Preparing Molybdenum Doped Titanium Dioxide Thin Film by Sol-Gel

Method for Preparing Molybdenum Doped Titanium Dioxide Thin Film by Sol-Gel

机译:溶胶凝胶法制备钼掺杂二氧化钛薄膜的方法

摘要

The present invention discloses a method for preparing molybdenum doped titanium dioxide thin film by sol-gel, comprising following steps: preparing a mixed solution containing tetrabutyl titanate, adding a thickener to obtain solution I, preparing solution II containing ammonium molybdate solution, dropwise adding solution II into solution I and obtaining a titanium dioxide sol; dipping the titanium dioxide sol on the surface of a glass ball and oven drying, repeating such for several times, removing a solvent by vacuum drying, carrying out high-temperature calcination, keeping warm and obtaining molybdenum doped titanium dioxide thin film. The molybdenum doped titanium dioxide thin film prepared by the present invention has higher specific surface area, and the catalyst after modeling deposition has better transmissivity and porosity, large reaction contact area, high light efficiency and good photocatalytic effect.
机译:本发明公开了一种溶胶-凝胶法制备钼掺杂的二氧化钛薄膜的方法,包括以下步骤:制备含钛酸四丁酯的混合溶液,加入增稠剂得到溶液I,制备含钼酸铵溶液的溶液II,滴加溶液于溶液II中加入二氧化钛并得到溶胶;将二氧化钛溶胶浸渍在玻璃球的表面上,并进行烘箱干燥,重复几次,通过真空干燥除去溶剂,进行高温煅烧,保持温热,得到钼掺杂的二氧化钛薄膜。本发明制备的掺钼二氧化钛薄膜具有较高的比表面积,模型沉积后的催化剂具有较好的透射率和孔隙率,反应接触面积大,光效率高,光催化效果好。

著录项

  • 公开/公告号US2017282159A1

    专利类型

  • 公开/公告日2017-10-05

    原文格式PDF

  • 申请/专利权人 YANCHENG INSTITUTE OF TECHNOLOGY;

    申请/专利号US201715405311

  • 申请日2017-01-13

  • 分类号B01J23/28;B01D53/86;B01J37/02;B01J37/08;B01J35;B01J37/04;

  • 国家 US

  • 入库时间 2022-08-21 13:50:54

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