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One-pot process for preparation of ammonium and hydroxyl ammonium derivatives of bis 5,5′-tetrazole-1,1′-dihydroxide
One-pot process for preparation of ammonium and hydroxyl ammonium derivatives of bis 5,5′-tetrazole-1,1′-dihydroxide
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机译:一锅法制备双5,5'-四唑-1,1'-二氢氧化铵的铵盐和羟基铵盐衍生物
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摘要
A one-pot process for preparing ammonium and hydroxylammonium salts of bis 5,5′-tetrazole-1,1′-dihydroxide, specifically, diammonium bis 5,5′-tetrazole-1,1′-diolate (ABTOX) and dihydroxylammonium 5,5′-bistetrazole-1,1′-diolate (TKX-50). The process requires the reaction of sodium azide, dichloroglyoxime, HCl in dioxane solution to form bis 5,5′-tetrazole-1,1′-dihydroxide and treating this product with either ammonium chloride to produce ABTOX or hydroxylamine hydrochloride to produce TKX-50.
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