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System and method for synthesis of POSS-graphene oxide derivatives as effective fillers for developing high performance composites

机译:合成POSS-氧化石墨烯衍生物作为开发高性能复合材料的有效填料的系统和方法

摘要

According to an embodiment, a method for grafting POSS (polyhedral silsesquioxane) nanomaterial to graphene oxide is described for use in preparation of high performance composite materials. In another embodiment, amine functionalized graphene oxide may be particularly suitable. In this embodiment, POSS molecules grafted to amine functionalized graphene oxide are synthesized by reacting graphene oxide with different POSS molecules. The amine functionalized graphene oxide may be dissolved in a solvent and the reaction may include the presence of a catalyst. The resultant POSS grafted graphene oxide/POSS grafted amine functionalized graphene oxide may be mixed with a resin (epoxy) in a masterbatch. The masterbatch may then be packaged and sold. The masterbatch material may then be introduced into the interlaminar area of graphite/epoxy composites. Biodegradability and interlaminar fracture toughness testing results from the use of epoxy based nanocomposites containing POSS modified graphene oxide polymer are expected to improve.
机译:根据一个实施方案,描述了一种用于将POSS(多面体倍半硅氧烷)纳米材料接枝到氧化石墨烯上的方法,用于制备高性能复合材料。在另一个实施方案中,胺官能化的氧化石墨烯可能是特别合适的。在该实施方案中,通过使氧化石墨烯与不同的POSS分子反应来合成接枝到胺官能化的氧化石墨烯上的POSS分子。可以将胺官能化的氧化石墨烯溶解在溶剂中,并且反应可以包括催化剂的存在。可以在母料中将所得的POSS接枝的氧化石墨烯/ POSS接枝的胺官能化的氧化石墨烯与树脂(环氧树脂)混合。然后可以将母料包装和出售。然后可以将母料材料引入石墨/环氧树脂复合材料的层间区域。预期使用包含POSS改性氧化石墨烯聚合物的环氧基纳米复合材料可改善生物降解性和层间断裂韧性测试结果。

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