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METHOD FOR PRODUCING A COMPONENT OF RARE EARTH METAL-DOPED QUARTZ GLASS

机译:稀土金属掺杂石英玻璃成分的制备方法

摘要

A method for producing a component with portions of a rare earth metal-doped quartz glass, an intermediate product containing voids and consisting of a SiO2 raw material doped with rare earth metal is introduced into a sinter mold the interior of which is bordered by a carbonaceous mold wall, and is melted therein into the component by gas pressure sintering at a maximum temperature above 1500° C. A shield is arranged between the mold wall and the intermediate product. In order to indicate a modified gas pressure sintering method that ensures the production of rare earth metal-doped quartz glass with reproducible properties, a bulk material of amorphous SiO2 particles with a layer thickness of at least 2 mm is used as the shield, the softening temperature thereof being at least 20° C. higher than the softening temperature of the doped SiO2 raw material, and the bulk material being gas-permeable at the beginning of the melting of the intermediate product, and the bulk material sintering during melting into an outer layer that is gas-tight to a pressure gas.
机译:将具有部分掺杂稀土金属的石英玻璃,包含空隙且由掺杂有稀土金属的SiO 2 原料组成的中间产品的部件的制造方法引入烧结模具中。其内部以碳质模具壁为边界,并通过在最高1500℃以上的最高温度下的气体压力烧结而在其中熔化成部件。在模具壁和中间产品之间布置有屏蔽。为了表明一种改进的气压烧结方法,该方法可确保生产具有可复制特性的掺稀土金属的石英玻璃,请使用层厚至少为2 mm的无定形SiO 2 颗粒的块状材料作为屏蔽层,其软化温度比掺杂的SiO 2 原料的软化温度高出至少20℃,并且块状材料在刚开始时是透气的。中间产物熔化,并且在熔化期间本体材料烧结成对压力气体不透气的外层。

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