首页> 外国专利> METHOD FOR SYNTHESIS OF A RADIOPAQUE SURFACE Ti-Ta-Ni ALLOY WITH AN AMORPHOUS OR AMORPHOUS-NANOCRYSTALLINE STRUCTURE ON TiNi ALLOY SUBSTRATE

METHOD FOR SYNTHESIS OF A RADIOPAQUE SURFACE Ti-Ta-Ni ALLOY WITH AN AMORPHOUS OR AMORPHOUS-NANOCRYSTALLINE STRUCTURE ON TiNi ALLOY SUBSTRATE

机译:TiNi合金基体上合成具有非晶态或非晶态-纳米晶结构的不透射线表面Ti-Ta-Ni合金的方法

摘要

FIELD: chemistry.;SUBSTANCE: invention relates to the chemical-pharmaceutical industry and is a method for synthesis of a radiopaque surface Ti-Ta-Ni alloy with an amorphous or amorphous-nanocrystalline structure on a TiNi alloy substrate, carried out by an additive method by repeated alternation in a single vacuum cycle of deposition operations of an amorphous film and its liquid-phase mixing with the substrate components, characterized in that a film of the Ti60-70Ta40-30 (at%) compound is used as an amorphous film deposited by simultaneous magnetron sputtering of targets from Ti and Ta, and subsequent liquid-phase mixing of the film and substrate components and high-speed quenching of a molten surface layer is carried out using a wide-aperture low-energy high-current electron beam (LEHCEP) with the parameters: pulse duration 2÷3 mcs, energy density 1.5÷2.5 J/cm2.;EFFECT: invention makes it possible to synthesize the surface Ti-Ta-Ni alloy with the amorphous or amorphous-nanocrystalline structure on the TiNi substrate with an increased level of radiopaque and thromboresistance.;6 cl, 6 dwg, 2 tbl, 4 ex
机译:化学领域本发明涉及化学制药工业,并且是一种通过添加剂在TiNi合金基底上合成具有非晶态或非晶态纳米晶结构的不透射线的表面Ti-Ta-Ni合金的方法。通过在单个真空循环中重复交替进行非晶膜的沉积操作及其与基底组分的液相混合的方法,其特征在于,Ti 60-70 Ta 40的膜-30 (at%)化合物被用作非晶膜,该膜通过同时磁控溅射Ti和Ta中的靶材,随后将膜和基材组分进行液相混合以及对熔融表面进行高速淬火来沉积使用宽孔径低能量大电流电子束(LEHCEP)进行镀层,其参数为:脉冲持续时间2÷3 mcs,能量密度1.5÷2.5 J / cm 2 。 :通过本发明,可以与金属表面合成Ti-Ta-Ni合金TiNi基体上的球形或无定形纳米晶体结构,具有不透射线和抗血栓形成的水平升高; 6 cl,6 dwg,2 tbl,4 ex

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