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METHOD OF PREPARING OIL SAMPLE FOR GAS CHROMATOGRAPHIC ANALYSIS OF LOW-VOLATILE POLAR SUBSTANCES

机译:低挥发性极性物质气相色谱分析的油样制备方法

摘要

FIELD: physics.;SUBSTANCE: invention relates to gas-chromatographic methods of analysing oil-soluble low-volatile polar compounds and can be used in oil and other industries for their quantitative determination. Low-volatile polar substances are extracted from oil in two stages. At the first stage low-volatile polar substances are extracted using a water-alcohol extracting agent (3:1). On the second one, they are concentrated using calcium chloride and pentanol-1, which in quantitative gas-chromatographic analysis simultaneously serves as an internal standard.;EFFECT: disclosed is a gas chromatographic method of analysing oil-soluble low volatile polar compounds.;1 cl, 1 dwg, 1 tbl
机译:发明领域本发明涉及分析油溶性低挥发性极性化合物的气相色谱方法,可用于石油和其他工业中进行定量测定。低挥发性极性物质分两个阶段从油中提取。在第一阶段,使用水醇萃取剂(3:1)萃取低挥发性极性物质。在第二种色谱柱上,将它们用氯化钙和戊醇-1浓缩,在定量气相色谱分析中同时用作内标。效果:公开了一种分析油溶性低挥发性极性化合物的气相色谱方法。 1厘升,1公升,1公吨

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