Process for in-situ synthesis of dispersion ZnO—TiO2 nanoparticles in oil

摘要

The present invention provides a process for in situ synthesis of dispersion of ZnO and TiO₂ nanoparticles in an oil medium, wherein the process comprises: (a) providing layered basic zinc hydroxide (LBZ) in an oil medium, containing a dispersant, (b) providing a titanium precursor in the oil medium to obtain a mixture, (c) hydrolyzing the mixture to obtain a suspension, and (d) decomposing the suspension to obtain a dispersion of mixture of ZnO and TiO₂ nanoparticles. The present invention also provides an oil dispersion comprising dispersant stabilized mixture of zinc oxide and titanium dioxide nanoparticles were synthesized through this process. The dispersion contains up to 2.5 Wt % metals loading balanced with dispersant and base oil or dispersant alone. Addition of this dispersion to oil of lubricating viscosity improves the anti-wear property and resulting a low SAPS formulation.