首页> 外国专利> ULTRATHIN NI-FE-MOF NANOSHEET, PREPARATION METHOD THEREFOR AND APPLICATION THEREOF

ULTRATHIN NI-FE-MOF NANOSHEET, PREPARATION METHOD THEREFOR AND APPLICATION THEREOF

机译:超薄镍-FE-MOF纳米片,制备方法及其应用

摘要

Provided is a preparation method for an ultrathin Ni-Fe-MOF nanosheet, comprising the following steps: dissolving an organic ligand in an organic solvent; dropwise adding the obtained solution into an aqueous solution with nickel salt and ferric salt dissolved; and mixing uniformly, and then reacting in a closed reaction kettle for 3-6 hours at 140-160°C, so as to obtain the ultrathin Ni-Fe-MOF nanosheet, wherein the organic ligand is p-phthalic acid and/or disodium terephthalate, and the organic solvent is N,N-dimethylacetamide and/or N,N-dimethylformamide. Also provided are an ultrathin Ni-Fe-MOF nanosheet and an application thereof. The preparation method needs no surfactant, and can synthesize a large quantity of 2D ultrathin MOF material. The product has a clean surface and is easy to clean.
机译:提供了一种超薄Ni-Fe-MOF纳米片的制备方法,包括以下步骤:将有机配体溶解在有机溶剂中;将有机配体溶解在有机溶剂中。将得到的溶液滴加到溶解有镍盐和铁盐的水溶液中。然后均匀混合,然后在密闭的反应釜中于140-160℃反应3-6小时,得到有机配体为对苯二甲酸和/或二钠的超薄Ni-Fe-MOF纳米片。对苯二甲酸酯,有机溶剂是N,N-二甲基乙酰胺和/或N,N-二甲基甲酰胺。还提供了超薄的Ni-Fe-MOF纳米片及其应用。该制备方法不需要表面活性剂,可以合成大量的二维超薄MOF材料。该产品表面清洁,易于清洁。

著录项

  • 公开/公告号WO2020073398A1

    专利类型

  • 公开/公告日2020-04-16

    原文格式PDF

  • 申请/专利权人 SOOCHOW UNIVERSITY;

    申请/专利号WO2018CN114307

  • 申请日2018-11-07

  • 分类号C07F19;C07F15/04;C25B11/06;C25B1/04;C08G83;

  • 国家 WO

  • 入库时间 2022-08-21 11:11:59

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