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MODEL AFM PROBE FOR OXIDIZED MINERAL COLLECTOR, PREPARATION METHOD AND APPLICATION THEREOF

机译:氧化矿物集合体的AFM模型探针,制备方法及其应用

摘要

#$%^&*AU2020100499A420200514.pdf#####ABSTRACT The present invention belongs to the technical field of force measurement and reagent preparation, and particularly relates to model atomic force measurement (AFM) probe for an oxidized mineral collector. The AFM probe includes a probe with a surface compounded with an Au layer, and a modified oxidized mineral collector, where the oxidized mineral collector is a compound having the structural formula: Y-A (Formula 1); Y is a hydrophobic group, which is an aromatic group, an alkane group or an olefin group; A is an active group, which is a carboxylic acid or a hydroxamic acid; the modified oxidized mineral collector modifies Y with -SH and forms a coordination compound from A and an M metal ion; the modified oxidized mineral collector is anchored on the Au layer of the probe by the -SH therein. The present invention further discloses a preparation method and an application of the probe. The present invention fills in a gap of direct force measurement between an oxidized mineral collector and a mineral in the prior art. The present invention directly measures the force between the reagent and the mineral surface with an accurate measurement method. 18DRAWINGS Pb2*-activated spodumene surface spodumene surface FIG. 1 . jSpodumene110) in 10'MKCISoluion, PH 8.0 25 Souee10il M.~l~o~H. 30. 25- b ~its 10- L -5 0 5 10 i5 20 25 30 10 15 20 25 30 35 AdhesioN/Radius, F_/R (mN~m) AdhesionRadius .,R(mN/n) FIG. 2
机译:#$%^&* AU2020100499A420200514.pdf #####抽象本发明属于测力和试剂技术领域制备方法,尤其涉及用于原子吸收光谱仪的模型原子力测量(AFM)探针氧化的矿物收集器。原子力显微镜探针包括一个表面与金属复合的探针金层和改性的氧化矿物收集器,其中氧化矿物收集器是具有结构式:Y-A的化合物(式1); Y是一个疏水基团,它是芳族基团,烷烃基或烯烃基; A是活性基团,是羧基酸或异羟肟酸;改性的氧化矿物捕收剂用-SH改性Y并形成来自A和M金属离子的配位化合物;改性的氧化矿物收集器是通过其中的-SH锚定在探针的Au层上。本发明进一步公开探针的制备方法和应用。本发明填补了直接的空白现有技术中氧化矿物收集器与矿物之间的压力测量。的本发明直接测量试剂与矿物表面之间的力。准确的测量方法。18岁图纸Pb2 *活化的锂辉石表面锂辉石表面图。 1个。 10'MKCl溶液中,pH 8.0 25 Souee10il M.〜l〜o〜H。30岁25-〜它10-大号-5 0 5 10 i5 20 25 30 10 15 20 25 30 35附着力N /半径,F_ / R(mN〜m)附着力半径。,R(mN / n)图。 2

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