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FURNACE BODY FOR THERMAL ANALYSIS INSTRUMENT AND THERMAL ANALYSIS INSTRUMENT PROVIDED WITH SAME

机译:用于热分析仪器的炉体和同时提供的热分析仪器

摘要

Provided are a furnace body for a thermal analysis instrument, which is capable of realizing rapid temperature rise and fall, and a thermal analysis instrument provided with the same, wherein, the furnace body comprises a hollow furnace main body (100), a heating system (90) and a refrigeration system (80) located below the furnace main body (100); the cross-section of the furnace main body (100) is dumbbell-shaped, two symmetrical sample cavities are provided inside the furnace main body (100), and a hole (7) is provided at the central portion as a ventilation channel for gas circulation in the cavity; the heating system (90) comprises two or more heat-conductive posts and two or more sets of heaters wrapped around the outer surface of the heat-conductive posts; the refrigeration system (80) comprises a hollow cold-conductive member (20) with one end being closed as a cold transfer surface (11) and the other end being open, a hollow refrigerant nozzle (19) that is nested inside the cold-conductive member (20) with a gap, a refrigerant inlet pipe (17) and a refrigerant outlet pipe (18) located at an open end side of a cooling guide (20), and a transition joint (23) respectively sealedly connected to the open end of the cold-conductive member (20) and the end of the refrigerant nozzle (19) away from the cold transfer surface (11); a plurality of heat-conductive posts are arranged below the two symmetrical sample cavities of the furnace main body (100) and are distributed in an axis symmetry; the heater includes heating wires symmetrically wrapped on the heat-conductive post; the inner wall of the refrigerant nozzle (19) and the transition joint (23) form a refrigerant inner cavity (81); the outer wall of the refrigerant nozzle (19) and the inner wall of the heat-conductive member (20) form a refrigerant outer cavity (82); the refrigerant inlet pipe (17) is in communication with the refrigerant inner cavity (81), and the refrigerant outlet pipe (18) is in communication with the refrigerant outer cavity (82).
机译:提供了一种能够实现温度的快速上升和下降的热分析仪用炉体以及具备该炉体的热分析仪,其中,炉体包括中空炉体(100),加热系统。 (90)和位于炉主体(100)下方的制冷系统(80);炉主体(100)的截面为哑铃状,在炉主体(100)的内部设有两个对称的样品腔,在中央部设有孔(7)作为气体的通气路。腔内循环;加热系统(90)包括两个或更多个导热柱以及围绕导热柱的外表面包裹的两组或更多组加热器。制冷系统(80)包括中空的冷媒部件(20),该中空的一端封闭为冷传递表面(11),而另一端是敞开的;中空的制冷剂喷嘴(19)嵌套在冷媒内部。带有间隙的导电部件(20),分别位于冷却引导件(20)的开口端侧的制冷剂入口管(17)和制冷剂出口管(18)以及过渡接头(23)分别密封地连接到所述导热部件(20)的开口端和所述制冷剂喷嘴(19)的远离所述冷媒表面(11)的端部。在炉主体100的两个对称的样品腔的下方配置有多个导热柱,并且多个导热柱以轴对称的方式分布。加热器包括对称缠绕在导热柱上的电热丝。制冷剂喷嘴(19)的内壁和过渡接头(23)形成制冷剂内腔(81)。制冷剂喷嘴(19)的外壁和导热部件(20)的内壁形成制冷剂外腔(82)。制冷剂入口管(17)与制冷剂内腔(81)连通,制冷剂出口管(18)与制冷剂外腔(82)连通。

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