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METHOD OF PRODUCING CELLULOSE

机译:纤维素的生产方法

摘要

FIELD: pulp and paper industry.;SUBSTANCE: invention relates to pulp-and-paper industry and can be used for production of cellulose and products based on it from non-wood vegetal raw materials. Method of producing cellulose involves delignification of milled vegetal raw material by boiling raw material at temperature of 85–90 °C in a solution of hydrogen peroxide in the presence of sulfuric acid and a catalyst, in form of molybdic acid salts, at the end of delignification extraction of residual oxidised lignin is performed, raw materials are represented by non-wood vegetal raw materials, and delignification of vegetal raw material is carried out with continuous thermomechanochemical activation of the delignification reaction mass by passing the reaction mass through the outer contour of the delignification capacity, equipped with an ultrasonic device or rotating anisotropic ferromagnetic bodies for 60–90 minutes, wherein the delignification solution contains hydrogen peroxide of 8 wt%, sulfuric acid 0.42 wt% and catalyst of sodium molybdate or ammonium molybdate 0.2 wt%, and extraction of residual oxidised lignin is carried out at temperature of 50 °C.;EFFECT: reduced time for production of cellulose from non-wood vegetal raw materials and reduced share of residual lignin in the end product.;1 cl, 3 dwg
机译:技术领域本发明涉及纸浆和造纸工业,可用于由非木质植物原料生产纤维素和基于纤维素的产品。纤维素的生产方法包括:通过在过硫酸氢盐和硫酸盐形式的催化剂存在下,在过氧化氢溶液中于85–90°C的温度下,将原料在85–90°C的温度下煮沸,将研磨后的植物原料脱木质素。进行残留的氧化木质素的脱木质素提取,原料以非木材植物原料为代表,通过使反应物质流过木质素的外部轮廓,通过脱木质素反应物质的连续热机械化学活化进行植物原料的脱木质素。脱木素能力,配备超声波装置或旋转各向异性铁磁体60-90分钟,其中脱木素溶液包含8 wt%的过氧化氢,0.42 wt%的硫酸和0.2 wt%的钼酸钠或钼酸铵催化剂,并进行萃取残留的氧化木质素在50°C的温度下进行;效果:减少了r从非木质植物原料生产纤维素,并减少最终产品中残留木质素的份额。; 1 cl,3 dwg

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