A practical synthesis of diethyl 1-methylthio-2-oxo-2-phenylethylphosphonates from diethyl methylthiomethylphosphonate

Rodrigues A.; Vinhato E.; Rittner R.; Olivato PR.

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A practical synthesis of diethyl 1-methylthio-2-oxo-2-phenylethylphosphonates from diethyl methylthiomethylphosphonate

机译：由二乙基甲基硫代甲基膦酸酯实际合成1-乙基硫基-2-乙基-2-氧代-2-苯基乙基膦酸二乙酯

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摘要

An efficient synthesis of 2'- and 3'-substituted diethyl 1-methylthio-2-oxo-2-phenylethylphosphonates 3a-k from 2'- and 3'-substituted benzoyl chlorides 2a-k using diethyl methylthio-l-lithiomethylphosphonate is described. [References: 34]

机译：描述了使用二乙基甲硫基-1-锂硫基甲基膦酸酯从2'-和3'-取代的苯甲酰氯2a-k有效合成2'-和3'-取代的1-乙基硫基-2-甲硫基-2-氧代-2-苯基乙基膦酸酯3a-k。。 [参考：34]

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《Synthesis: International Journal of Methods in Synthetic Organic Chemistry》 |2003年第8期|共5页
作者
Rodrigues A.; Vinhato E.; Rittner R.; Olivato PR.;
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正文语种 eng
中图分类有机化学;
关键词
Diethyl 1-methylthio-2-oxo-2-phenylethylphosphonates; Diethyl methylthiomethylphosphonate; Michaelis-arbuzov reaction; Acylation reaction; Beta-keto phosphonates; Triethyl phosphonoacetate; Carbonyl phosphonates; Ketophosphonates; Phosphite; Acid; 2-aryl-2-oxoalkylphosphonates; Acylation; Chlorides; Reagents;

机译：1-甲基硫代-2-氧代-2-膦酸二乙酯;甲基硫代甲基二膦酸乙酯;Michaelis-arbuzov反应;酰化反应;β-酮基膦酸酯;膦酸三乙酯;羰基膦酸酯;酮膦酸酯;亚磷酸酯;酸;2-芳基-2-氧代烷基膦酸酯;酰化;氯化物;试剂;

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1. A practical synthesis of diethyl 1-methylthio-2-oxo-2-phenylethylphosphonates from diethyl methylthiomethylphosphonate [J] . Rodrigues A., Vinhato E., Rittner R., Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2003,第8期

机译：由二乙基甲基硫代甲基膦酸酯实际合成1-乙基硫基-2-乙基-2-氧代-2-苯基乙基膦酸二乙酯
2. A fast and practical synthesis of tert-butyl esters from 2-tert-butoxypyridine using boron trifluoride center dot diethyl etherate under mild conditions [J] . Minh Thanh La, Kim Hee-Kwon Tetrahedron . 2018,第27期

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机译：2-二乙基 - 和2-二异丙基氨基乙磺酸的合成

A practical synthesis of diethyl 1-methylthio-2-oxo-2-phenylethylphosphonates from diethyl methylthiomethylphosphonate

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