Trichloroisocynuric Acid/DMF as Efficient Reagent for Chlorodehydration of Alcohols Under Conventional and Ultrasonic Conditions

Venkana Purugula; Kumar Mukka Satish; Rajanna Kamatala Chinna; Ali Mir Moazzam

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Trichloroisocynuric Acid/DMF as Efficient Reagent for Chlorodehydration of Alcohols Under Conventional and Ultrasonic Conditions

机译：三氯异氰尿酸/ DMF作为常规和超声条件下醇氯去水合的有效试剂

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摘要

A new and efficient method for the chlorodehydration of alcohols utilizing TCCA/DMF is described. Various alcohols can be converted smoothly into their corresponding alkyl chlorides in high yields under mild conditions with short reaction times.

机译：描述了一种利用TCCA / DMF对醇进行氯脱水的新有效方法。各种醇可以在温和的条件下以短的反应时间以高收率平稳地转化为它们相应的烷基氯。

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来源
《Synthesis and reactivity in inorganic, metal-organic, and nano-metal chemistry》 |2015年第3期|共7页
作者
Venkana Purugula; Kumar Mukka Satish; Rajanna Kamatala Chinna; Ali Mir Moazzam;
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正文语种 eng
中图分类化学反应的机理和动力学;非金属元素及其化合物;元素有机化合物;特种结构材料;
关键词
Alcohols; alkyl chlorides; chlorodehydration; N; N dimethyl formamide; sonication; trichloroisocyanuric acid;

机译：醇;烷基氯;氯脱水;N;N二甲基甲酰胺;超声处理;三氯异氰尿酸;

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1. Trichloroisocynuric Acid/DMF as Efficient Reagent for Chlorodehydration of Alcohols Under Conventional and Ultrasonic Conditions [J] . Venkana Purugula, Kumar Mukka Satish, Rajanna Kamatala Chinna, Synthesis and reactivity in inorganic, metal-organic, and nano-metal chemistry . 2015,第1a3期

机译：三氯异氰尿酸/ DMF作为常规和超声条件下醇氯去水合的有效试剂
2. Efficient and chemoselective alkylation of amines/amino acids using alcohols as alkylating reagents under mild conditions [J] . Chu-Pei Xu, Zhen-Hua Xiao, Bi-Qin Zhuo, Chemical Communications . 2010,第41期

机译：在温和条件下使用醇作为烷基化试剂，对胺/氨基酸进行高效和化学选择性烷基化
3. Wet Carbon-Based Solid Acid/Potassium Bromate as an Efficient Heterogeneous Reagent for Oxidation of Alcohols under Mild Conditions [J] . Synthetic Communications . 2008,第7期

机译：湿碳基固体酸/溴酸钾作为温和条件下酒精氧化的高效多相试剂
4. Highly Efficient Synthesis of Allenyltitanium Reagents Propargyl Alcohol Derivatives.Practical Synthesis of Homopargyl Alcohols [C] . Fang-Long Yang International symposium for Chinese organic chemists . 2000

机译：高效合成亚甲硝基试剂炔丙醇衍生物。常卤醇的实际合成
5. Approaches to the total synthesis of (+/-)-pseudomonic acids. Model studies and reagent development in stereo- and regiocontrolled Pd-catalyzed alkylations and arylations of allylic alcohol derivatives. [D] . Brescia, Marc-Raleigh. 1997

机译：（+/-）-假单仲酸的全合成方法。立体和区域控制的Pd催化烯丙基醇衍生物的烷基化和芳基化的模型研究和试剂开发。
6. Bacteriophage Mediates Efficient Gene Transfer in Combination with Conventional Transfection Reagents [O] . Amanda Donnelly, Teerapong Yata, Kaoutar Bentayebi, 2015

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7. Efficient and chemoselective alkylation of amines/amino acids using alcohols as alkylating reagents under mild conditions [O] . Xu Chu-Pei, Xiao Zhen-Hua, Zhuo Bi-Qin, 2010

机译：在温和条件下使用醇作为烷基化试剂，对胺/氨基酸进行高效和化学选择性烷基化

Trichloroisocynuric Acid/DMF as Efficient Reagent for Chlorodehydration of Alcohols Under Conventional and Ultrasonic Conditions

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