Linear viscoelastic studies on a transient network formed by host–guest interaction

Kashiwagi Yu; Katashima Takuya; Nakahata Masaki; Takashima Yoshinori; Harada Akira; Inoue Tadashi

摘要

ABSTRACT > A host–guest (HG) polymer was prepared through the radical polymerization of acrylamide monomers (AAm) with a small amount of host‐guest linkers, β‐cyclodextrin‐attached AAm (βCD‐AAm) and adamantane‐attached AAm (Ad‐AAm). The linear viscoelastic and swelling measurements indicated that the resulting HG polymer swollen in water was gel‐like, although the HG polymer is conceptually a linear chain having only temporary crosslinkings. NMR measurements indicated that half of the βCD units incorporated in the HG polymer do not form the inclusion complex with Ad. Rheological analysis of the HG polymer revealed that HG interaction retarded the Rouse modes of networks but did not affect the level of the plateau modulus, which was simply described by the entanglements of AAm chains. This result was confirmed with the reference experiment, in which Ad were capped by competitive βCD molecules. Furthermore, the PAAm polymer with only βCD units (no Ad) was found to exhibit gel‐like behavior. This behavior was attributed to the formation of a small amount of rotaxane structure, which act as permanent crosslinkings, based on 2D NMR data. The HG polymer is basically an entanglement network with temporary sticky points due to the HG interaction, and a few permanent branching points. ? 2018 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2018 , 56 , 1109–1117 </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns=”http://www.wiley.com/namespaces/wiley“type=”main“><title type=”main“>摘要>通过丙烯酰胺单体（AAm）与少量主客体连接物、β-环糊精连接的AAm（βCD-AAm）和金刚烷连接的AAm（Ad-AAm）的自由基聚合制备了主客体（HG）聚合物线性粘弹性和溶胀测量结果表明，在水中溶胀的HG聚合物呈凝胶状，尽管HG聚合物在概念上是仅具有临时交联的线性链。核磁共振测量表明，HG聚合物中一半的βCD单元不会与Ad形成包合物。HG聚合物的流变学分析表明，HG相互作用延缓了网络的Rouse模式，但不会影响平台模量的水平，这可以简单地用AAm链的缠结来描述。参考实验证实了这一结果，在该实验中，Ad被竞争性βCD分子封端。此外，仅含有βCD单元（无Ad）的PAAm聚合物表现出凝胶状行为。根据2D NMR数据，这种行为归因于少量轮烷结构的形成，其作为永久性交联。汞聚合物基本上是一个缠结网络，由于汞的相互作用，有临时的粘滞点和一些永久的分支点？2018威利期刊有限公司J.Polym。Sci。，B部分：理工大学。菲斯 2018年，56，1109-1117</abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-35627/'>《Journal of Polymer Science, Part B. Polymer Physics》</a> <b style="margin: 0 2px;">|</b><span>2018年第15期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kashiwagi Yu&option=202" target="_blank" rel="nofollow">Kashiwagi Yu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Katashima Takuya&option=202" target="_blank" rel="nofollow">Katashima Takuya;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nakahata Masaki&option=202" target="_blank" rel="nofollow">Nakahata Masaki;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Takashima Yoshinori&option=202" target="_blank" rel="nofollow">Takashima Yoshinori;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Harada Akira&option=202" target="_blank" rel="nofollow">Harada Akira;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Inoue Tadashi&option=202" target="_blank" rel="nofollow">Inoue Tadashi;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of Macromolecular Science Graduate School of ScienceOsaka UniversityToyonaka Osaka 560‐0043 Japan;</p> <p>Department of Macromolecular Science Graduate School of ScienceOsaka UniversityToyonaka Osaka 560‐0043 Japan;</p> <p>Department of Materials Engineering Science Graduate School of Engineering ScienceOsaka UniversityToyonaka Osaka 560‐8531 Japan;</p> <p>Department of Macromolecular Science Graduate School of ScienceOsaka UniversityToyonaka Osaka 560‐0043 Japan;</p> <p>Department of Macromolecular Science Graduate School of ScienceOsaka UniversityToyonaka Osaka 560‐0043 Japan;</p> <p>Department of Macromolecular Science Graduate School of ScienceOsaka UniversityToyonaka Osaka 560‐0043 Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1185.html" title="高分子化学（高聚物）">高分子化学（高聚物）;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=host–guest interaction&option=203" rel="nofollow">host–guest interaction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=supramolecular network&option=203" rel="nofollow">supramolecular network;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=viscoelasticity&option=203" rel="nofollow">viscoelasticity;</a> </p> <div class="translation"> 机译：主客互动;超分子网络;粘弹性; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-journal-cn_chinese-chemical-letters_thesis/0201271485063.html">Advances in the study of the host-guest interaction by using coronene as the guest molecule</a> <b>[J]</b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Jianqiao Li&option=202" target="_blank" rel="nofollow" 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Pluth,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=*&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">* </a> <span>-1</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：线性自由能关系显示结构氢键主客体相互作用的变化</span> </p> </li> <li> <div> <b>12. </b><a class="enjiyixqcontent" href="/open-access_resources_thesis/010007093105.html ">Supramolecular polymer hydrogels induced by host–guest interactions with di-[cyclobis(paraquat-p-phenylene)] cross-linkers: from molecular complexation to viscoelastic properties</a> <b>[O] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fumagalli, Matthieu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Fumagalli, Matthieu,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Belal, Khaled&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Belal, Khaled,</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Guo, Hui&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Guo, Hui,</a> <span>2017</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：主客体与双[[环双（百草枯-对苯撑）]交联剂的客体相互作用诱导的超分子聚合物水凝胶：从分子络合到粘弹性</span> </p> </li> <li> <div> <b>13. </b><a class="enjiyixqcontent" href="/ntis-science-report_de_thesis/02071208360.html">Dynamical Study of Guest-Host Orientational Interaction in Liquid Crystalline Materials Doctoral thesis</a> <b>[R] </b> . <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Truong, T. V.&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">Truong, T. V. </a> <span>2005</span> </span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：液晶材料中客体 - 主体取向相互作用的动力学研究博士论文</span> </p> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-31709_thesis/02022421018.html">A Theoretical Study on the Molecular Recognition of Cyclodextrins with Guests in Ground and Excited States</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ke-sheng Song&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . Ke-sheng Song</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lei Liu&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Lei Liu</a> <span> <a href="/conference-cn-31709/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十二届全国光化学学术讨论会 </a> <span> <span> . 2001</span> </span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020312396416.html">Enhanced Spray Retention of Droplets by Host-Guest Interaction Based Surfactants Using Pillar[5]Arene</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=O ADITHYA DANANJAYA PADMAPERUMA&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . O ADITHYA DANANJAYA PADMAPERUMA</a> <span> . 2018</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06130408567424.html">- - COMPOSITION FOR FORMING GUEST-HOST POLARIZER AND GUEST-HOST POLARIZER COMPRISING THE SAME</a> <b>[P]</b> . <span> 外国专利：  KR101768191B1 </span> <span> . 2017-08-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：--形成客座极化器和组成相同的客座极化器的组合 </span> </p> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06130408567423.html">- - COMPOSITION FOR FORMING GUEST-HOST POLARIZER AND GUEST-HOST POLARIZER COMPRISING THE SAME</a> <b>[P]</b> . <span> 外国专利：  KR101768192B1 </span> <span> . 2017-08-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：--形成客座极化器和组成相同的客座极化器的组合 </span> </p> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130408549409.html">- - COMPOSITION FOR FORMING GUEST-HOST POLARIZER AND GUEST-HOST POLARIZER COMPRISING THE SAME</a> <b>[P]</b> . <span> 外国专利：  KR101786571B1 </span> <span> . 2017-10-18</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：--形成客座极化器和组成相同的客座极化器的组合 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" 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