Observations on the reaction of nitronate anions with oxalyl chloride: a new method for the preparation of geminal chloronitroso compounds

Rafael Bou-Moreno; Sandra Luengo-Arratta; William B. Motherwell

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Observations on the reaction of nitronate anions with oxalyl chloride: a new method for the preparation of geminal chloronitroso compounds

机译：亚硝酸根阴离子与草酰氯反应的观察：一种制备双氯亚硝基化合物的新方法

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摘要

A simple method for the preparation of geminal chloronitroso compounds from secondary nitro compounds via their derived nitronate anions is presented.

机译：提出了一种简单的方法，可通过仲硝基化合物通过其衍生的亚硝酸根阴离子制备双氯亚硝基化合物。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2011年第17期|共3页
作者
Rafael Bou-Moreno; Sandra Luengo-Arratta; William B. Motherwell;
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正文语种 eng
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关键词
Chloronitroso; Hetero Diels-Alder; Oxalyl chloride; Nitronate anion;

机译：亚氯酸;杂Diels-Alder;草酰氯;亚硝酸根阴离子;

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1. Observations on the reaction of nitronate anions with oxalyl chloride: a new method for the preparation of geminal chloronitroso compounds [J] . Rafael Bou-Moreno, Sandra Luengo-Arratta, William B. Motherwell Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2011,第17期

机译：亚硝酸根阴离子与草酰氯反应的观察：一种制备双氯亚硝基化合物的新方法
2. Reactions of 1-haloadamantanes and ethylmercury chloride with nitronate anions by the S(RN)1 mechanism [J] . Santiago AN, Basso SM, Toledo CA, New Journal of Chemistry . 2005,第7期

机译：通过S（RN）1机理研究1-重金刚烷和氯化乙基汞与亚硝酸根阴离子的反应
3. 1,1-Cycloaddition of Oxalyl Dichloride with Dialkenyl metal Compounds:Formation of Cyclopentadienone Derivatives by the Reaction of 1,4,-Dilithio-1,3-dienes or Zirconacyclopentadienes with Oxalyl Chloride in the Presence of CuCl [J] . Chao Chen, Chanjuan Xi, Yanfeng Jiang, Journal of the American Chemical Society . 2005,第22期

机译：草酰二氯与二烯基金属化合物的1,1-环加成反应：在CuCl存在下，1,4，-二硫代1,3-二烯或氧化锆环戊二烯与草酰氯反应形成环戊二烯酮衍生物
4. Studies on The Reactions of Cyclic Oxalyl Compounds with Oxindole and Lawesson Reagent [C] . Elif KORKUSUZ, Ismail YILDIRIM European Symposium on Organic Chemistry . 2009

机译：氧吲哚和法律试剂的环状氧基氧基化合物的反应研究
5. PREPARATION AND REACTIONS OF ANIONS DERIVED FROM PENTABORANE(9); PREPARATION OF NEW METALLABORANES (BORANES, HEXABORANE(10)) [D] . WERMER, JOSEPH RAYMOND. 1986

机译：戊硼烷衍生的阴离子的制备和反应（9）;制备新的金属硼烷（硼烷，六硼烷（10））
6. Metabolism of polycyclic compounds. 17. The reaction of 1:2-dihydronaphthalene and 1:2-epoxy-1:2:3:4-tetrahydronaphthalene with glutathione catalysed by tissue preparations [O] . J. Booth, E. Boyland, T. Sato, 1960

机译：多环化合物的代谢。 17.1：2-二氢萘和1：2-环氧-1：2：3：4-四氢萘与组织制剂催化的谷胱甘肽的反应
7. 1, 1-Cycloaddition of Oxalyl Dichloride with Dialkenylmetal Compounds: Formation of Cyclopentadienone Derivatives by the Reaction of 1, 4, -Dilithio-1, 3-dienes or Zirconacyclopentadienes with Oxalyl Chloride in the Presence of CuCl [O] . -1

机译：1,1-环加二氯乙烯与二烷基金矿化合物的环加成：通过在CuCl存在下通过1,4，-dilithiO-1，3-二烯或锆氰基化苯甲酸锆或锆氰基化萘乙烷的反应形成环戊二烯酮衍生物
8. Observation of Dihalide Elimination Upon Electron Attachment to Oxalyl Chloride and Oxalyl Bromide, 300-550 K [R] . Van Doren, J. M. , Hogan, K. B. , Miller, T. M. , 2006

机译：电子附着于草酰氯和草酰溴上的双卤素消除观察，300-550 K

Observations on the reaction of nitronate anions with oxalyl chloride: a new method for the preparation of geminal chloronitroso compounds

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