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Synthesis of titania-coated silica nanoparticles using ono-ionic water-in-oil

机译:离子油包水合成二氧化钛包覆的二氧化硅纳米粒子

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Titania (TiO2) nanocoating on silica (SiO2) particles was obtained by controlled hydrolysis of titanium alkoxide precursors. Monodisperse spherical silica particles prepared by Stober method were used as the support. Isolated silica particles with uniform titania nanocoating were obtained by reacting appropriate alkoxide and water at ambient temperature. The thickness and uniformity of TiO2 coating were controlled by adjusting the concentrations of reactants and the amount of added SiO2. The samples were characterized using electron microscopy and electrophoresis. The surface coverage was estimated using isoelectric point (IEP) data. (C) 2001 Elsevier Science B.V. All rights reserved. [References: 18]
机译:通过对烷氧基钛前体进行可控水解获得了二氧化硅(SiO2)颗粒上的二氧化钛(TiO2)纳米涂层。通过Stober方法制备的单分散球形二氧化硅颗粒用作载体。通过使适当的醇盐与水在环境温度下反应,获得具有均匀的二氧化钛纳米涂层的分离的二氧化硅颗粒。通过调节反应物的浓度和SiO 2的添加量来控制TiO 2涂层的厚度和均匀性。使用电子显微镜和电泳对样品进行表征。使用等电点(IEP)数据估算表面覆盖率。 (C)2001 Elsevier Science B.V.保留所有权利。 [参考:18]

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