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Comparison of yield, composition, and antioxidant activity of turmeric (Curcuma longa L.) extracts obtained using various techniques

机译:比较使用各种技术获得的姜黄提取物的产量,组成和抗氧化活性

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Turmeric extracts were obtained from two lots of raw material (M and S) using various techniques: hydrodistillation, low pressure solvent extraction, Soxhlet, and supercritical extraction using carbon dioxide and cosolvents. The solvents and cosolvents tested were ethanol, isopropyl alcohol, and their mixture in equal proportions. The composition of the extracts was determined by gas chromatography-flame ionization detection (GC-FID) and UV. The largest yield (27%, weight) was obtained in the Soxhlet extraction (turmeric (S), ethanol = 1:100); the lowest yield was detected in the hydrodistillation process (2.1%). For the supercritical extraction, the best cosolvent was a mixture of ethanol and isopropyl alcohol. Sixty percent of the light fraction of the extracts consisted of ar-turmerone, (Z)-gamma-atlantone, and (E)-gamma-atlantone, except for the Soxhlet extracts (1:100, ethanol), for which only ar-turmeronol and (Z)-alpha-atlantone were detected. The maximum amount of curcuminoids (8.43%) was obtained using Soxhlet extraction (ethanol/isopropyl alcohol). The Soxhlet and low pressure extract exhibited the strongest antioxidant activities.
机译:姜黄提取物是使用多种技术从两种原料(M和S)中获得的:加氢蒸馏,低压溶剂萃取,索氏萃取以及使用二氧化碳和助溶剂的超临界萃取。测试的溶剂和助溶剂为乙醇,异丙醇及其相等比例的混合物。通过气相色谱-火焰电离检测(GC-FID)和紫外线确定提取物的组成。在索氏提取中获得最大的收率(27%,重量)(姜黄(S),乙醇= 1:100);在加氢蒸馏过程中,收率最低(2.1%)。对于超临界萃取,最好的助溶剂是乙醇和异丙醇的混合物。萃取物中60%的轻质馏分由ar-turmerone,(Z)-γ-丙二酮和(E)-γ-丙二酮组成,但索氏提取物(1:100,乙醇)除外,其中只有ar-检出了松油醇和(Z)-α-大西洋蛋白。使用索氏提取法(乙醇/异丙醇)可获得最大量的姜黄素(8.43%)。索氏提取物和低压提取物表现出最强的抗氧化活性。

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