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Preparation and properties of quartz cloth-reinforced Xylok composites fabricated by vacuum bag only process

机译:真空袋法制备石英布增强Xylok复合材料的制备及性能

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摘要

Xylok resin was synthesized from 1,4-bis(methoxymethyl)-benzene and phenol through a condensation reaction catalyzed by p-toluenesulfonic acid. The effects of molar ratio of phenol to 1,4-bis(methoxymethyl)-benzene, reaction time and washing process on the properties of Xylok resin were investigated. Xylok composite laminates reinforced by quartz cloth were fabricated by vacuum bag only (VBO) process. Softening point of Xylok resin and volatile content of prepreg and voids in composites were also studied to better control process defects in composite laminates. Void content was measured by image analysis and calculating parameters. Experimental results showed that the Xylok composite laminates manufactured by VBO process had good thermal and dielectric properties. The flexural strength and flexural modulus of laminates could be 733 MPa and 23 GPa, respectively.
机译:Xylok树脂是由1,4-双(甲氧基甲基)苯与苯酚通过对甲苯磺酸催化的缩合反应合成的。研究了苯酚与1,4-双(甲氧基甲基)苯的摩尔比,反应时间和洗涤工艺对木酚醛树脂性能的影响。石英布增强的Xylok复合层压板是通过仅真空袋(VBO)工艺制造的。还研究了Xylok树脂的软化点以及复合材料中预浸料和空隙的挥发物含量,以更好地控制复合材料层压板中的工艺缺陷。通过图像分析和计算参数测量空隙含量。实验结果表明,采用VBO工艺生产的Xylok复合层压板具有良好的热和介电性能。层压板的弯曲强度和弯曲模量分别为733 MPa和23 GPa。

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