X-ray powder diffraction data for acetamidinium formate C3H8N2O2, elimination of preferred orientation effect

摘要

X-ray powder diffraction data, unit-cell parameters, and space group for acetamidinium formate, C3H8N2O2, are reported [a = 6.4564(5) angstrom, c = 13.021 (3) angstrom, unit-cell volume V = 542.8(3) angstrom(3), M.p. = 215(1)degrees C, rho(c) =1.274 g.cm(-3), rho(m) = 1.269 g.cm(-3), Z = 4, and space group P(43)2(1)2]. The front loaded technique got sample with strong preferred orientation because of plate-like shape of crystallites, so the capillary packing was used for final powder data collection. All measured lines were indexed and are consistent with the P4(3)2(1)2 space group. No detectable impurities were observed. (C) 2017 International Centre for Diffraction Data.