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Characterization of silver sulfide nanoparticles synthesized by a simple precipitation method

机译:简单沉淀法合成的硫化银纳米粒子的表征

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摘要

Silver sulfide nanoparticles with different sizes were synthesized using a simple aqueous precipitation. Particles were obtained in the presence of three stabilizing agents controlling thus particle size and agglomeration. The particles obtained were characterized using XRD, scanning electron microscopy (SEM), transmission electron microscopy (TEM), thermal and spectroscopy techniques. We observed a "size quantization" effect reflected in a shift on the band gap value of smaller sample obtained.
机译:使用简单的水沉淀法合成了不同尺寸的硫化银纳米颗粒。在三种稳定剂的存在下获得颗粒,所述稳定剂控制了粒径和团聚。使用XRD,扫描电子显微镜(SEM),透射电子显微镜(TEM),热学和光谱学技术对获得的颗粒进行表征。我们观察到“大小量化”效应反映在所获得的较小样本的带隙值偏移上。

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