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Preparation and characterization of ceria nanoparticles using crystalline hydrate cerium propionate as precursor

机译:以结晶水合丙酸铈为前驱体制备二氧化铈纳米粒子及其表征

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摘要

Ceria nanoparticles were synthesized simply by pyrolysis method using hydrate cerium propionate as precursor. The effect of pyrolysis temperature on the physical properties of ceria was investigated. It was found that the large crystals of precursor cracked to many nano-sized ceria particles on heating, and the medium particle sizes D_(50) determined by laser scattering (LS) method decreased firstly and then increased with minimum value around 460 nm at calcination temperature of 1000 ℃. SEM observations showed that the average particle size of synthesized ceria powders ranged from 20 to 50 nm.
机译:以水合丙酸铈为前驱体,通过热解法简单地合成了二氧化铈纳米颗粒。研究了热解温度对二氧化铈物理性质的影响。研究发现,前驱体的大晶体在加热时会破裂成许多纳米级的二氧化铈颗粒,通过激光散射(LS)法测定的中等粒径D_(50)在煅烧时首先减小,然后在460nm附近以最小值增加。温度1000℃。 SEM观察显示,合成的二氧化铈粉末的平均粒径为20至50nm。

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