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Influence of V_2O_5 additions on the permeability and power loss characteristics of Ni-Zn ferrites

机译:V_2O_5添加量对Ni-Zn铁氧体磁导率和功率损耗特性的影响

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摘要

Poly crystalline nickel-zinc ferrites with the chemical formula, Ni_(0.65)Zn_(0.35)Fe_2O_4+x V_2O_5, where x values range from 0.0 to 1.5 wt.% in steps of 0.3 wt.%, have been prepared by conventional ceramic technique. The samples were sintered for 4 h in air at 1210 ℃. The XRD analyses of the samples confirm single phase cubic spinel structures. Micrographs of the materials reveal that vanadium additions resulted in fine grain structures with small pores trapped inside the grains as the vanadium concentration increases. Complex permeability of these ferrites exhibit stable frequency responses up to 7 MHz beyond which the real part decreases sharply and the imaginary part increases to have a peak at the relaxation frequency. Power loss has been found to be quite low for these materials up to 3 MHz, thereafter it increases steeply due to large eddy current losses. The results are explained in terms of the compositional and microstructural modifications brought about by the vanadium additions.
机译:已经通过常规陶瓷技术制备了化学式为Ni_(0.65)Zn_(0.35)Fe_2O_4 + x V_2O_5的多晶镍锌铁氧体,其中x值范围为0.0到1.5 wt。%,步长为0.3 wt。%。 。将样品在空气中于1210℃烧结4小时。样品的XRD分析证实了单相立方尖晶石结构。材料的显微照片表明,钒的添加会导致细晶粒结构,随着钒浓度的增加,晶粒内部会捕获小孔。这些铁氧体的复磁导率在高达7 MHz的频率范围内表现出稳定的频率响应,超过此频率,实部急剧减小,虚部增大,在弛豫频率处出现峰值。对于这些材料,已经发现功率损耗在3 MHz以下是非常低的,此后由于大的涡流损耗,功率损耗急剧增加。用钒的添加引起的组成和微观结构的改变来解释结果。

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