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Analysis of the microstructure and phase constitution of the Fe_3Al/18-8 diffusion interface after re-heating

机译:再加热后Fe_3Al / 18-8扩散界面的微观结构和相组成分析

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The existence of coarse precipitation blocked the diffusion of the atoms and caused the uneven distribution of elements at the Fe_3 Al/18-8 interface zone. Especially, the brittle precipitation could induce welding cracks directly. Consequently, it was one of the main factors that caused the failure of the joint. The Fe_3 Al/18-8 diffusion-bonded joint was re-heated and the precipitation and phase constitution of the interface were analysed by means of scanning electron microscope (SEM), energy dispersive spectrum (EDS) and X-ray diffraction (XRD). The results indicated that the precipitation became tiny and regular and distributed evenly due to re-heating. The brittle precipitation zone was liquified to become a smooth and homogeneous diffusion zone. There were no high-microhardness brittle phases such as FeAl_2 and Fe_2Al_5 near the Fe_3Al/18-8 diffusion interface after re-heating.
机译:粗大析出物的存在阻止了原子的扩散,并导致元素在Fe_3 Al / 18-8界面区域的分布不均匀。特别是,脆性沉淀可直接引起焊接裂纹。因此,这是导致关节破坏的主要因素之一。加热Fe_3 Al / 18-8扩散结合接头,并通过扫描电子显微镜(SEM),能量色散谱(EDS)和X射线衍射(XRD)分析界面的沉淀和相组成。结果表明,由于重新加热,降水变得微细且规则,并且分布均匀。脆性沉淀区被液化成光滑均匀的扩散区。再加热后,在Fe_3Al / 18-8扩散界面附近没有高显微硬度的脆性相,如FeAl_2和Fe_2Al_5。

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