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Microstructure and sliding wear behavior of pure titanium surface modified by double-glow plasma surface alloying with Nb

机译:Nb二次辉光等离子体表面合金改性的纯钛表面的组织和滑动磨损行为

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摘要

In the present work, a Ti-Nb alloyed layer was successfully formed on the pure titanium surface by double-glow plasma surface alloying technology with Nb and the wear resistance has been investigated. The microstructure, phase identification and elements distribution were analyzed by optical microscope (OM), scanning electron microscope (SEM), energy dispersive spectrometer (EDS) and X-ray powder diffraction (XRD). Specified tribological characterization was carried out by using a ball-on-disc tribometer and MicroXAM Surface Mapping Microscope at room temperature. The nano-hardness of the alloyed layer was also improved from 3.25 GPa to 5.25 GPa. As compared with pure titanium substrate, the friction coefficient of the alloyed layer was reduced from 0.57 to 0.27. The wear volume and relative wear rate at room temperature were reduced by 82% and 86%, which corresponded to an improvement of wear resistance. In the Haemolysis test, the treated sample exhibited better biocompatibility. Measuring the anodic polarization curves in Tyrode's solution, the treated sample indicated a decreased corrosion rate.
机译:在目前的工作中,利用含Nb的双辉光等离子体表面合金化技术成功地在纯钛表面上形成了Ti-Nb合金层,并研究了其耐磨性。通过光学显微镜(OM),扫描电子显微镜(SEM),能量色散光谱仪(EDS)和X射线粉末衍射(XRD)分析了显微组织,相识别和元素分布。通过在室温下使用圆盘球式摩擦计和MicroXAM表面测绘显微镜进行指定的摩擦学表征。合金层的纳米硬度也从3.25 GPa提高到5.25 GPa。与纯钛基底相比,合金层的摩擦系数从0.57降低至0.27。室温下的磨损量和相对磨损率分别降低了82%和86%,这与耐磨性的提高相对应。在溶血试验中,处理过的样品表现出更好的生物相容性。测量蒂罗德溶液中的阳极极化曲线,处理后的样品表明腐蚀速率降低。

著录项

  • 来源
    《Materials & design》 |2013年第12期|265-273|共9页
  • 作者单位

    College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211100, China;

    College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211100, China;

    College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211100, China;

    College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211100, China;

    College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211100, China;

    AVIC Landing Gear Advanced Manufacturing Corp, Changsha 410200, China;

    AVIC Landing Gear Advanced Manufacturing Corp, Changsha 410200, China;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Pure titanium surface; Surface alloying; Microstructure; Wear resistance;

    机译:纯钛表面;表面合金化;微观结构耐磨性;

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