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Rapid detection of adulteration of milks from different species using Fourier Transform Infrared Spectroscopy (FTIR)

机译:使用傅立叶变换红外光谱(FTIR)快速检测不同种类的牛奶的掺假

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摘要

The aim of the studies reported in the Research Communication was to develop a rapid spectro-scopic technique as an alternative method for the classification and discrimination of milk sources by Fourier transform infrared spectroscopy (FTIR). Cow, sheep and water buffalo milk samples were collected from various local milk producers in Istanbul, Turkey. In addition, various brands of packaged milk were purchased locally. Spectrums were obtained according to milk species origin and binary mixtures prepared in increments of 10% (10, 20, 30, 40, 50, 60, 70, 80 and 90%) for each sample analysed in FTIR spectroscopy. A successful milk species (cow, sheep, and water buffalo) discrimination and classification were achieved utilising Hierarchical cluster and principle component analyses (PCA) on the basis of Euclidean distance and Ward's algorithm. Amide-I (1700-1600/cm) and Amide-ll (1565-1520/cm) spectral bands were used in the che-mometric method. The results of the study indicated that adulteration of milk samples can be quantitatively detected by the FTIR technique in a short time with high accuracy. In conclusion, this method could be used as a new alternative technique for routine analysis in authenticity control of milk species origin.
机译:《研究通讯》中报道的研究目的是开发一种快速光谱技术,作为通过傅立叶变换红外光谱(FTIR)对牛奶来源进行分类和区分的替代方法。牛,绵羊和水牛牛奶样品是从土耳其伊斯坦布尔的多家当地牛奶生产商那里采集的。此外,在当地购买了各种品牌的包装牛奶。根据牛奶种类来源和以FTIR光谱法分析的每个样品以10%的增量(10%,20%,30%,40%,50%,60%,70%,80%和90%)制备的二元混合物获得光谱。在欧几里德距离和沃德算法的基础上,使用层次聚类和主成分分析(PCA)成功实现了牛奶种类(牛,绵羊和水牛)的区分和分类。化学测定法中使用了酰胺I(1700-1600 / cm)和酰胺II(1565-1520 / cm)的光谱带。研究结果表明,可以通过FTIR技术在短时间内高精度地定量检测牛奶样品的掺假情况。综上所述,该方法可作为常规分析奶种来源真实性的常规分析方法。

著录项

  • 来源
    《Journal of dairy research》 |2018年第2期|222-225|共4页
  • 作者单位

    Faculty of Chemistry-Metallurgy, Department of Food Engineering, Yildiz Technical University, 34210, Istanbul, Turkey;

    Faculty of Chemistry-Metallurgy, Department of Food Engineering, Yildiz Technical University, 34210, Istanbul, Turkey,Department of Food Engineering, Faculty of Engineering and Architecture, Mus Alparslan University, 49100, Mus, Turkey;

    Faculty of Chemistry-Metallurgy, Department of Food Engineering, Yildiz Technical University, 34210, Istanbul, Turkey;

  • 收录信息 美国《科学引文索引》(SCI);美国《生物学医学文摘》(MEDLINE);美国《化学文摘》(CA);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    FTIR; milks; classification; adulteration; chemometrics;

    机译:FTIR;牛奶分类;掺假化学计量学;

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