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Effect of aluminide coatings on penetration and microstructure of TIG welded 9Cr-1Mo steel for fusion blanket applications

机译:铝化物涂层对TIG焊接9Cr-1Mo熔覆层应用的熔深和组织的影响

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Aluminide coatings with a top alumina layer on 9Cr steels are considered candidates for fusion blanket applications. One of the critical issues associated with such coating is the fabrication sequence. It is therefore important to investigate the effect of aluminide coating on weld properties of 9Cr steels. This work is a preliminary investigation of the weldability of aluminide coated 9Cr-1Mo steels using bead-on-plate welding experiments. Alumina coated GRADE 91 steel samples by hot dip aluminizing followed by normalizing and plasma tempering were generated. Bead-on-plate welding studies were conducted at different heat inputs by varying the weld speed (100,125,150 mm/min) and using a constant current of 200A by autogenous tungsten inert gas (TIG) welding process. The effect of coating on the weld microstructure was investigated using X-ray diffraction (XRD), scanning electron microscopy with energy dispersive x-rays (SEM-EDX) and microhardness tests. It was observed that the presence of alumina (Al2O3) on the top of coated samples resulted in improved depth of penetration (DOP) due to arc constriction. The presence of Al rich inclusions (AlN) in the weld bead were also observed. The marginal increase in Al concentration of the weld bead appears to reduce the grain size of weld metal for coated sample and microhardness was enhanced compared to the uncoated 9Cr-1Mo steels.
机译:在9Cr钢上具有顶部氧化铝层的铝化物涂层被认为是融合毯应用的候选材料。与这种涂层相关的关键问题之一是制造顺序。因此,重要的是研究铝化物涂层对9Cr钢焊接性能的影响。这项工作是通过珠焊法对镀铝9Cr-1Mo钢的可焊性进行的初步研究。通过热浸渗铝,然后进行正火和等离子回火,生成了氧化铝涂层的GRADE 91钢样品。通过改变焊接速度(100,125,150 mm / min)并通过自生钨极惰性气体(TIG)焊接使用200A恒定电流,在不同的热量输入下进行了串焊焊接研究。使用X射线衍射(XRD),带有能量色散X射线的扫描电子显微镜(SEM-EDX)和显微硬度测试研究了涂层对焊缝微观结构的影响。观察到,由于电弧收缩,在涂覆样品的顶部存在氧化铝(Al2O3)导致渗透深度(DOP)的改善。还观察到焊缝中富铝夹杂物(AlN)的存在。与未涂层的9Cr-1Mo钢相比,焊道中Al浓度的边际增加似乎减小了涂层样品的焊接金属的晶粒尺寸,并且提高了显微硬度。

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