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Microstructural evolution, mechanical properties, and corrosion resistance of a heat-treated Mg alloy for the bio-medical application

机译:生物医学应用热处理镁合金的微观组织演变,力学性能和耐腐蚀性

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During the recent years, some Mg based alloys have extensively been considered as a new generation of degradable and absorbable bio-medical materials. In this work, the Mg–2Zn–1Gd–1Ca (wt%) alloy as a new metallic bio-material was produced by the casting process followed by the heat treatment. The samples of the alloy were solution treated at temperatures of 500, 550, and 600?°C and then quench aged at temperatures of 125, 150, and 175?°C. The results of SEM-EDS examinations indicated that the alloy microstructure consists of α-Mg matrix and the Ca2Mg6Zn3and Mg3Gd2Zn3secondary phases. With regard to the results of Vickers hardness test, the temperatures of 500?°C and 150?°C were selected as the optimum solutionizing and aging temperatures, respectively. Moreover, the dissolution of casting precipitates and production of lattice distortion occurring after the solution treatment led to the reduction in ultimate shear strength up to 21%. But, the precipitation hardening and morphological changes taking place during the aging treatment improved the ultimate shear strength up to 32%. Furthermore, the results of electro-chemical and weight-loss measurements in a simulated body fluid indicated that the heat-treated alloy is a promising candidate for the Mg based alloys recently considered for the bio-medical applications.
机译:近年来,一些镁基合金被广泛认为是新一代可降解和可吸收的生物医学材料。在这项工作中,Mg–2Z​​n–1Gd–1Ca(wt%)合金是一种新的金属生物材料,它是通过铸造工艺随后进行热处理而制成的。合金样品在500、550和600?C的温度下进行固溶处理,然后在125、150和175?C的温度下淬火。 SEM-EDS检测结果表明,合金的微观组织由α-Mg基体和Ca2Mg6Zn3和Mg3Gd2Zn3第二相组成。关于维氏硬度测试的结果,分别选择500℃和150℃的温度作为最佳固溶温度和时效温度。此外,固溶处理后铸件析出物的溶解和晶格变形的产生导致极限抗剪强度降低多达21%。但是,时效处理过程中发生的沉淀硬化和形态变化将最终的剪切强度提高了32%。此外,在模拟体液中进行电化学和失重测量的结果表明,经热处理的合金是最近被考虑用于生物医学应用的Mg基合金的有前途的候选者。

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