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Small angle neutron scattering and small angle X-ray scattering studies of platinum-loaded carbon foams

机译:载铂碳泡沫的小角中子散射和小角X射线散射研究

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The morphology of carbon nanofoam samples comprising platinum nanoparticles dispersed in the matrix was characterized by small angle neutron scattering (SANS) and small angle X-ray scattering (SAXS) techniques. Results show that the structure of pores of carbon matrix exhibits a mass (pore) fractal nature and the average radius of the platinum particles is about 2.5 nm. The fractal dimension as well as the size distribution parameters of platinum particles varies markedly with the platinum content and annealing temperature. Transmission electron micrographs of the samples corroborate the SANS and SAXS results.
机译:通过小角度中子散射(SANS)和小角度X射线散射(SAXS)技术表征了包含分散在基质中的铂纳米粒子的碳纳米泡沫样品的形貌。结果表明,碳基体的孔结构具有质量(孔隙)分形的性质,铂颗粒的平均半径约为2.5 nm。铂粒子的分形维数和尺寸分布参数随铂含量和退火温度而显着变化。样品的透射电子显微照片证实了SANS和SAXS结果。

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