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Creep in Al Single Crystal Processed by Equal-channel Angular Pressing

机译:等通道角挤压铝单晶的蠕变

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n this work the creep behavior and microstructure changes in aluminum single crystal during equal-channel angular pressing (ECAP) were investigated in order to understand the relationships between microstructure and creep behavior. The investigated crystal was oriented with {111} parallel to the shear plane and was parallel to the direction of shear. During ECAP by route A at room temperature single-crystalline sample was subsequently transformed into the polycrystalline material. Microstructure of samples processed by 1 and 4 ECAP passes was characterized by transmission electron microscope (TEM) and scanning electron microscope (SEM) equipped with the electron backscatter diffraction unit (EBSD). Microstructure analyses showed inhomogeneity of microstructure after ECAP and the increase in the fraction of of HAGB's (θ>15°) with increasing number of ECAP passes. Tensile creep tests at temperature of 373K and at applied stress of 50 MPa were performed on the Al single crystal after one and four ECAP passes. It was found that the creep behavior is influenced by cooperative grain boundary sliding along mesoscopic shear bands.
机译:在这项工作中,研究了铝单晶在等通道转角挤压(ECAP)期间的蠕变行为和微观结构变化,以了解微观结构与蠕变行为之间的关系。所研究的晶体的取向是{111}平行于剪切平面,并且平行于剪切方向。在室温下通过路线A进行ECAP期间,随后将单晶样品转化为多晶材料。通过透射电子显微镜(TEM)和配备电子背散射衍射单元(EBSD)的扫描电子显微镜(SEM)对经过1和4次ECAP通道处理的样品的微观结构进行了表征。显微组织分析显示,随着ECAP通过次数的增加,ECAP后显微组织不均匀,HAGB的分数(θ> 15°)增加。经过一到四次ECAP之后,对Al单晶进行了373K温度和50 MPa施加应力的拉伸蠕变测试。发现蠕变行为受沿介观剪切带的协同晶界滑动影响。

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