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Breaking Preconceptions: Thin Section Petrography For Ceramic Glaze Microstructures

机译:打破先入之见:陶瓷釉微结构的薄截面岩石学

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During the last thirty years, microstructural and technological studies on ceramic glazes have been essentially carried out through the use of Scanning Electron Microscopy (SEM) combined with energy dispersive X-ray analysis (EDX). On the contrary, optical microscopy (OM) has been considered of limited use in solving the very complex and fine-scale microstructures associated with ceramic glazes. As the crystallites formed inside glazes are sub- and micrometric, a common misconception is that it is not possible to study them by OM. This is probably one of the reasons why there are no available articles and textbooks and even no visual resources for describing and characterizing the micro-crystallites formed in glaze matrices. A thin section petrography (TSP) for ceramic glaze microstructures does not exist yet, neither as a field of study nor conceptually. In the present contribution, we intend to show new developments in the field of ceramic glaze petrography, highlighting the potential of OM in the microstructural studies of ceramic glazes using petrographic thin sections. The outcomes not only stress the pivotal role of thin section petrography for the study of glaze microstructures but also show that this step should not be bypassed to achieve reliable readings of the glaze microstructures and sound interpretations of the technological procedures. We suggest the adoption by the scientific community of an alternative vision on glaze microstructures to turn thin section petrography for glaze microstructures into a new specialized petrographic discipline. Such an approach, if intensively developed, has the potential to reduce the time and costs of scientific investigations in this specific domain. In fact, it can provide key reference data for the identification of the crystallites in ceramic glazes, avoiding the repetition of exhaustive protocols of expensive integrated analyses.
机译:在过去的三十年中,通过使用扫描电子显微镜(SEM)结合能量色散X射线分析(EDX)基本上对陶瓷釉进行了微结构和技术研究。相反,光学显微镜(OM)被认为在解决与陶瓷釉相关的非常复杂和精细的微观结构方面用途有限。由于釉料内部形成的微晶是亚微米和微米级的,因此常见的误解是无法通过OM研究它们。这可能是为什么没有可用的文章和教科书,甚至没有视觉资源来描述和表征釉基质中形成的微晶的原因之一。陶瓷釉微结构的薄截面岩石学(TSP)尚不存在,既不是研究领域,也不是概念上的研究。在当前的贡献中,我们打算展示陶瓷釉岩岩石学领域的新发展,强调OM在使用岩石学薄截面的陶瓷釉体微观结构研究中的潜力。研究结果不仅强调了薄片岩石学在研究釉微结构方面的关键作用,而且还表明,不应绕过这一步骤来获得对釉微结构的可靠读数和对工艺流程的合理解释。我们建议科学界采用一种对釉料微结构的替代性观点,以将用于釉料微结构的薄截面岩石学变成一门新的专门岩石学学科。如果大力开发这种方法,则有可能减少该特定领域的科学研究时间和成本。实际上,它可以为陶瓷釉料中的微晶鉴定提供关键的参考数据,从而避免了重复进行昂贵的综合分析的详尽协议。

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